(6aR,9R)-7-Phenethyl-4,6,6a,7,8,9-hexahydro-indolo[4,3-fg]quinoline-9-carboxylic acid diethylamide

Base Information

Chemical Name:(6aR,9R)-7-Phenethyl-4,6,6a,7,8,9-hexahydro-indolo[4,3-fg]quinoline-9-carboxylic acid diethylamide
CAS No.:96930-88-0
Molecular Formula:C₂₇H₃₁N₃O
Molecular Weight:413.563
Hs Code.:

Synonyms:(6aR,9R)-7-Phenethyl-4,6,6a,7,8,9-hexahydro-indolo[4,3-fg]quinoline-9-carboxylic acid diethylamide

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Chemical Property of (6aR,9R)-7-Phenethyl-4,6,6a,7,8,9-hexahydro-indolo[4,3-fg]quinoline-9-carboxylic acid diethylamide

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Technology Process of (6aR,9R)-7-Phenethyl-4,6,6a,7,8,9-hexahydro-indolo[4,3-fg]quinoline-9-carboxylic acid diethylamide

There total 3 articles about (6aR,9R)-7-Phenethyl-4,6,6a,7,8,9-hexahydro-indolo[4,3-fg]quinoline-9-carboxylic acid diethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 103-63-9
1-phenyl-2-bromoethane

: 35779-43-2
8β-6-norlysergic acid diethylamide

: 96930-88-0
(6aR,9R)-7-Phenethyl-4,6,6a,7,8,9-hexahydro-indolo[4,3-fg]quinoline-9-carboxylic acid diethylamide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 25 ℃; for 120h;
DOI:10.1021/jm00147a022

Reference yield:

: 35779-41-0
9,10-didehydro-N,N-diethyl-6-cyanoergoline-8β-carboxamide

: 96930-88-0
(6aR,9R)-7-Phenethyl-4,6,6a,7,8,9-hexahydro-indolo[4,3-fg]quinoline-9-carboxylic acid diethylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / Zn / acetic acid; H₂O / 4 h / Heating

2: 85 percent / K₂CO₃ / dimethylformamide / 120 h / 25 °C

With potassium carbonate; zinc; In water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00147a022

Reference yield:

: 50-37-3
lysergide

: 96930-88-0
(6aR,9R)-7-Phenethyl-4,6,6a,7,8,9-hexahydro-indolo[4,3-fg]quinoline-9-carboxylic acid diethylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / CCl₄; CHCl₃ / 6 h / Heating

2: 61 percent / Zn / acetic acid; H₂O / 4 h / Heating

3: 85 percent / K₂CO₃ / dimethylformamide / 120 h / 25 °C

With potassium carbonate; zinc; In tetrachloromethane; chloroform; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00147a022