Methyl-4,6-di-O-(4-methoxybenzylidene)-2,3-di-O-benzoyl-α-D-glucopyranoside

Base Information

Chemical Name:Methyl-4,6-di-O-(4-methoxybenzylidene)-2,3-di-O-benzoyl-α-D-glucopyranoside
CAS No.:273397-25-4
Molecular Formula:C29H28 O9
Molecular Weight:520.536
Hs Code.:
Mol file:273397-25-4.mol

Synonyms:Methyl-4,6-di-O-(4-methoxybenzylidene)-2,3-di-O-benzoyl-α-D-glucopyranoside

Suppliers and Price of Methyl-4,6-di-O-(4-methoxybenzylidene)-2,3-di-O-benzoyl-α-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
METHYL-2,3-DI-O-BENZOYL-4,6-O-(4-METHOXYBENZYLIDENE)-ALPHA-D-GLUCOPYRANOSIDE 95.00%
5MG
$ 505.63

Total 3 raw suppliers

Chemical Property of Methyl-4,6-di-O-(4-methoxybenzylidene)-2,3-di-O-benzoyl-α-D-glucopyranoside

Chemical Property:

Boiling Point:646.1±55.0 °C(Predicted)
PSA：98.75000
Density:1.33±0.1 g/cm3(Predicted)
LogP:3.93170

Purity/Quality:

97% ^*data from raw suppliers

METHYL-2,3-DI-O-BENZOYL-4,6-O-(4-METHOXYBENZYLIDENE)-ALPHA-D-GLUCOPYRANOSIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Methyl-4,6-di-O-(4-methoxybenzylidene)-2,3-di-O-benzoyl-α-D-glucopyranoside

There total 2 articles about Methyl-4,6-di-O-(4-methoxybenzylidene)-2,3-di-O-benzoyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 98-88-4
benzoyl chloride

: 185754-26-1
(2S,4aR,7R,8R,8aR)-6-methoxy-2-(4-methoxyphenyl)hexahydropyrano[3,2-d][1,3]dioxine-7,8-diol

: 273397-25-4
methyl 2,3-di-O-benzoyl-4,6-O-(4-methoxybenzylidene)-α-D-galactopyranoside

Guidance literature:: With pyridine; at 20 ℃; for 12h;
DOI:10.1016/S0957-4166(00)00212-3

Reference yield: 73.0%

: 93-97-0
benzoic acid anhydride

: 185754-26-1
(2S,4aR,7R,8R,8aR)-6-methoxy-2-(4-methoxyphenyl)hexahydropyrano[3,2-d][1,3]dioxine-7,8-diol

: C₂₂H₂₄O₈

: 273397-25-4
methyl 2,3-di-O-benzoyl-4,6-O-(4-methoxybenzylidene)-α-D-galactopyranoside

Guidance literature:: With 2,4,6-trimethyl-pyridine; copper(II) trifluoroacetate; In acetonitrile; at 20 ℃; for 6h; regioselective reaction;
DOI:10.1080/07328303.2014.996291

Reference yield: 67.0%

: 273397-25-4
methyl 2,3-di-O-benzoyl-4,6-O-(4-methoxybenzylidene)-α-D-galactopyranoside

: 273397-26-5
methyl 2,3-di-O-benzoyl-6-O-(4-methoxybenzyl)-α-D-galactopyranoside

Guidance literature:: With 4 A molecular sieve; sodium cyanoborohydride; trifluoroacetic acid; In N,N-dimethyl-formamide; at 20 ℃; for 7h;
DOI:10.1016/S0957-4166(00)00212-3