4-methoxybenzyl 5-chloro-1-cyclopropyl-6,7-bis((4-methoxybenzyl)oxy)-4-oxo-1,4-dihydroquinolin-3-carboxylate

Base Information

Chemical Name:4-methoxybenzyl 5-chloro-1-cyclopropyl-6,7-bis((4-methoxybenzyl)oxy)-4-oxo-1,4-dihydroquinolin-3-carboxylate
CAS No.:1429440-04-9
Molecular Formula:C₃₇H₃₄ClNO₈
Molecular Weight:656.132
Hs Code.:

Synonyms:4-methoxybenzyl 5-chloro-1-cyclopropyl-6,7-bis((4-methoxybenzyl)oxy)-4-oxo-1,4-dihydroquinolin-3-carboxylate

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Chemical Property of 4-methoxybenzyl 5-chloro-1-cyclopropyl-6,7-bis((4-methoxybenzyl)oxy)-4-oxo-1,4-dihydroquinolin-3-carboxylate

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Technology Process of 4-methoxybenzyl 5-chloro-1-cyclopropyl-6,7-bis((4-methoxybenzyl)oxy)-4-oxo-1,4-dihydroquinolin-3-carboxylate

There total 8 articles about 4-methoxybenzyl 5-chloro-1-cyclopropyl-6,7-bis((4-methoxybenzyl)oxy)-4-oxo-1,4-dihydroquinolin-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1429440-03-8
5-chloro-1-cyclopropyl-6,7-dihydroxy-4-oxo-1,4-dihydroquinolin-3-carboxylic acid

: 824-94-2
p-methoxybenzyl chloride

: 1429440-04-9
4-methoxybenzyl 5-chloro-1-cyclopropyl-6,7-bis((4-methoxybenzyl)oxy)-4-oxo-1,4-dihydroquinolin-3-carboxylate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 5h; Inert atmosphere;

Reference yield:

: 138998-46-6
ethyl 3-(dimethylamino)-2-(2,4,5-trifluorobenzoyl)prop-2-enoate

: 1429440-04-9
4-methoxybenzyl 5-chloro-1-cyclopropyl-6,7-bis((4-methoxybenzyl)oxy)-4-oxo-1,4-dihydroquinolin-3-carboxylate

Guidance literature:: Multi-step reaction with 7 steps

1.1: diethyl ether; ethanol / 2 h / 20 °C / Inert atmosphere

1.2: 2 h / 100 °C / Inert atmosphere

2.1: water; potassium hydroxide / 48 h / 130 °C / Inert atmosphere

3.1: sulfuric acid; potassium nitrate / 0 - 20 °C / Inert atmosphere

4.1: sodiumsulfide nonahydrate; water / ethanol / 2 h / 100 °C / Inert atmosphere

5.1: hydrogenchloride; sodium nitrite / water / 7 h / 0 - 95 °C / Inert atmosphere

6.1: methanol; boron tribromide / dichloromethane / -78 - 20 °C / Inert atmosphere

7.1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 50 °C / Inert atmosphere

With hydrogenchloride; methanol; sodiumsulfide nonahydrate; sulfuric acid; water; boron tribromide; potassium carbonate; potassium nitrate; potassium hydroxide; sodium nitrite; In diethyl ether; ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1429440-00-5
1-cyclopropyl-6,7-dimethoxy-5-nitro-4-oxo-1,4-dihydroquinolin-3-carboxylic acid

: 1429440-04-9
4-methoxybenzyl 5-chloro-1-cyclopropyl-6,7-bis((4-methoxybenzyl)oxy)-4-oxo-1,4-dihydroquinolin-3-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: sodiumsulfide nonahydrate; water / ethanol / 2 h / 100 °C / Inert atmosphere

2: hydrogenchloride; sodium nitrite / water / 7 h / 0 - 95 °C / Inert atmosphere

3: methanol; boron tribromide / dichloromethane / -78 - 20 °C / Inert atmosphere

4: potassium carbonate / N,N-dimethyl-formamide / 5 h / 50 °C / Inert atmosphere

With hydrogenchloride; methanol; sodiumsulfide nonahydrate; water; boron tribromide; potassium carbonate; sodium nitrite; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;