triethylaluminum diethyl ether adduct

Base Information

• Chemical Name: triethylaluminum diethyl ether adduct
• CAS No.: 879678-94-1
• Molecular Formula: C₇H₁₉AlO
• Molecular Weight: 146.209

Synonyms:triethylaluminum diethyl ether adduct

Chemical Property of triethylaluminum diethyl ether adduct

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of triethylaluminum diethyl ether adduct

There total 2 articles about triethylaluminum diethyl ether adduct which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethyl ether (60-29-7,927820-24-4) + tris(pentafluorophenyl)aluminum*(toluene)0.5 + trimethylaluminum (75-24-1) → Al(CH3)2(C6F5)*(C2H5)2O (219627-08-4) + Al(CH3)(C6F5)2*(C2H5)2O (219627-07-3) + trimethyl-alane; compound with diethyl ether (879678-94-1)

Guidance literature:

In ⁽²⁾H₈-toluene; 20°C; detd. by NMR spectroscopy;

DOI:10.1021/om980400j

Reference yield:

diethyl ether (60-29-7,927820-24-4) + Al2(C6F5)3(CH3)3 → triethylaluminum diethyl ether adduct (879678-94-1) + (C6F5)3Al*O(C2H5)2 tris-(pentafluoro phenyl) alane etherate + AlC6F5(CH3)2O(C2H5)2 + Al(C6F5)2CH3O(C2H5)2

Guidance literature:

excess of Et2O;

DOI:10.1021/om000573k

Reference yield:

triethylaluminum diethyl ether adduct (879678-94-1) → diethyl ether (60-29-7,927820-24-4) + trimethylaluminum (75-24-1)

Guidance literature:

thermal dissociation, above 373 K; products not isolated, reaction monitoring by pressure measurement; Kinetics;

upstream raw materials:

diethyl ether

trimethylaluminum

Downstream raw materials:

diethyl ether

trimethylaluminum

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