3,3'-bis(dimethylamino)azoxybenzene

Base Information

• Chemical Name: 3,3'-bis(dimethylamino)azoxybenzene
• CAS No.: 21232-52-0
• Molecular Formula: C₁₆H₂₀N₄O
• Molecular Weight: 284.361
• Mol file: 21232-52-0.mol

Synonyms:3,3'-bis(dimethylamino)azoxybenzene

Chemical Property of 3,3'-bis(dimethylamino)azoxybenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,3'-bis(dimethylamino)azoxybenzene

There total 8 articles about 3,3'-bis(dimethylamino)azoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

N,N-dimethyl-3-nitroaniline (619-31-8) → 3,3'-bis(dimethylamino)azoxybenzene (21232-52-0)

Guidance literature:

With methanol; potassium hydroxide; In toluene; for 21h; Heating;

Reference yield: 60.8%

N,N-dimethyl-3-nitroaniline (619-31-8) → 3,3'-bis(dimethylamino)azoxybenzene (21232-52-0) + m-dimethylaminoaniline (2836-04-6)

Guidance literature:

With potassium isopropoxide; In isopropyl alcohol; at 75 ℃;

DOI:10.1039/P29860001419

Reference yield:

methanol (67-56-1) + N,N-dimethyl-3-nitroaniline (619-31-8) → 3,3'-bis(dimethylamino)azoxybenzene (21232-52-0)

Guidance literature:

With sodium; at 100 ℃; schliesslich auf 125grad;

upstream raw materials:

methanol

N,N-dimethyl-3-nitroaniline

N,N-dimethyl-aniline

Refernces

• 1、 Prato, Maurizio,Quintily, Ugo,Scapol, Lucia,Scorrano, Gianfranco. "The synthesis of anilines or azoxybenzenes from the reduction of nitrobenzenes in basic alcoholic media". . p. 99 - 102. Retrieved 2007/10/02.