Benzyl-3,4-<<(O-benzylglycino)carbonyl>(cyan)methylen>-3,4-didesoxy-α-D-arabinopyranosid

Base Information

Chemical Name:Benzyl-3,4-<<(O-benzylglycino)carbonyl>(cyan)methylen>-3,4-didesoxy-α-D-arabinopyranosid
CAS No.:135468-90-5
Molecular Formula:C₂₄H₂₄N₂O₆
Molecular Weight:436.464
Hs Code.:

Synonyms:Benzyl-3,4-<<(O-benzylglycino)carbonyl>(cyan)methylen>-3,4-didesoxy-α-D-arabinopyranosid

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Chemical Property of Benzyl-3,4-<<(O-benzylglycino)carbonyl>(cyan)methylen>-3,4-didesoxy-α-D-arabinopyranosid

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Technology Process of Benzyl-3,4-<<(O-benzylglycino)carbonyl>(cyan)methylen>-3,4-didesoxy-α-D-arabinopyranosid

There total 3 articles about Benzyl-3,4-<<(O-benzylglycino)carbonyl>(cyan)methylen>-3,4-didesoxy-α-D-arabinopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 2462-31-9
benzyl 2-aminoacetate hydrochloride

: 135468-89-2
Benzyl 3,4-(C-cyano-carboxy)methano-3,4-dideoxy-α-D-arabinopyranoside

: 135468-90-5
Benzyl-3,4-<<(O-benzylglycino)carbonyl>(cyan)methylen>-3,4-didesoxy-α-D-arabinopyranosid

Guidance literature:: With 4-methyl-morpholine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; In N,N-dimethyl-formamide; for 6h;

Reference yield:

: 71204-45-0
benzyl 2,3-anhydro-4-O-trifluoromethanesulfonyl-β-L-ribopyranoside

: 135468-90-5
Benzyl-3,4-<<(O-benzylglycino)carbonyl>(cyan)methylen>-3,4-didesoxy-α-D-arabinopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / NaH / tetrahydrofuran / 1.) 0 deg C, 10 min, 2.) 0 deg C, 20 min

2: 98 percent / CF₃COOH / CH₂Cl₂ / 0.5 h

3: 66 percent / dimethylformamide / 6 h

With sodium hydride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 135468-86-9
Benzyl-3,4-<(tert-butoxycarbonyl)cyanmethylen>-3,4-didesoxy-α-D-arabinopyranosid

: 135468-90-5
Benzyl-3,4-<<(O-benzylglycino)carbonyl>(cyan)methylen>-3,4-didesoxy-α-D-arabinopyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / CF₃COOH / CH₂Cl₂ / 0.5 h

2: 66 percent / dimethylformamide / 6 h

With trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;