diethyl 2,2-((pentane-3,3-diylbis(2-methyl-4,1-phenylene))bis(oxy))diacetate

Base Information

Chemical Name:diethyl 2,2-((pentane-3,3-diylbis(2-methyl-4,1-phenylene))bis(oxy))diacetate
CAS No.:1416802-52-2
Molecular Formula:C₂₇H₃₆O₆
Molecular Weight:456.579
Hs Code.:

Synonyms:diethyl 2,2-((pentane-3,3-diylbis(2-methyl-4,1-phenylene))bis(oxy))diacetate

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Chemical Property of diethyl 2,2-((pentane-3,3-diylbis(2-methyl-4,1-phenylene))bis(oxy))diacetate

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Technology Process of diethyl 2,2-((pentane-3,3-diylbis(2-methyl-4,1-phenylene))bis(oxy))diacetate

There total 1 articles about diethyl 2,2-((pentane-3,3-diylbis(2-methyl-4,1-phenylene))bis(oxy))diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 55041-27-5
3,3-bis[4-hydroxy-3-methylphenyl]pentane

: 105-36-2
ethyl bromoacetate

: 1416802-51-1
ethyl 2-(4-(3-(4-hydroxy-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)acetate

: 1416802-52-2
diethyl 2,2-((pentane-3,3-diylbis(2-methyl-4,1-phenylene))bis(oxy))diacetate

Guidance literature:: 3,3-bis[4-hydroxy-3-methylphenyl]pentane; With sodium hydride; In N,N-dimethyl-formamide; paraffin oil; at 20 ℃; for 2h; Inert atmosphere;

ethyl bromoacetate; In N,N-dimethyl-formamide; paraffin oil; for 16h; Inert atmosphere;

Reference yield: 25.0%

: 1416802-52-2
diethyl 2,2-((pentane-3,3-diylbis(2-methyl-4,1-phenylene))bis(oxy))diacetate

: 1416802-53-3
2-(4-(3-(4-(2-ethoxy-2-oxoethoxy)-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)acetic acid

Guidance literature:: With lithium hydroxide monohydrate; In tetrahydrofuran; methanol; at 20 ℃; for 16h; Inert atmosphere;

Reference yield:

: 1416802-52-2
diethyl 2,2-((pentane-3,3-diylbis(2-methyl-4,1-phenylene))bis(oxy))diacetate

: 1416802-69-1
ethyl 2-(4-(3-(4-(2-hydroxyethoxy)-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide monohydrate / tetrahydrofuran; methanol / 16 h / 20 °C / Inert atmosphere

2: borane-THF / tetrahydrofuran / 19 h / -10 - 20 °C / Inert atmosphere

With borane-THF; lithium hydroxide monohydrate; In tetrahydrofuran; methanol;