2,6-dibromo-9-(3-O-acetyl-5-O-benzoyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-9H-purine

Base Information

Chemical Name:2,6-dibromo-9-(3-O-acetyl-5-O-benzoyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-9H-purine
CAS No.:134217-12-2
Molecular Formula:C₁₉H₁₅Br₂FN₄O₅
Molecular Weight:558.158
Hs Code.:

Synonyms:2,6-dibromo-9-(3-O-acetyl-5-O-benzoyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-9H-purine

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Chemical Property of 2,6-dibromo-9-(3-O-acetyl-5-O-benzoyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-9H-purine

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Technology Process of 2,6-dibromo-9-(3-O-acetyl-5-O-benzoyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-9H-purine

There total 2 articles about 2,6-dibromo-9-(3-O-acetyl-5-O-benzoyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-9H-purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.6%

: 1083-48-3
4-Nitrobenzylpyridin

: 3742-81-2
1-ethylcyclohexyl acetate

: 56632-81-6
1,3-di-O-acetyl-5-O-benzoyl-2-deoxy-2-fluoro-D-arabinofuranosyl bromide

: 134217-12-2
2,6-dibromo-9-(3-O-acetyl-5-O-benzoyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-9H-purine

Guidance literature:: silica gel; In 1,1-dichloroethane;

Reference yield: 31.6%

: 56632-81-6
1,3-di-O-acetyl-5-O-benzoyl-2-deoxy-2-fluoro-D-arabinofuranosyl bromide

: 1196-41-4
2,6-dibromopurine

: 134217-12-2
2,6-dibromo-9-(3-O-acetyl-5-O-benzoyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-9H-purine

: 137648-19-2
2,6-dibromo-9-(3-O-acetyl-5-O-benzoyl-2-deoxy-2-fluoro-α-D-arabinofuranosyl)-9H-purine

Guidance literature:: With 4 A molecular sieve; In 1,2-dichloro-ethane; at 100 ℃; for 32h;
DOI:10.1021/jm00080a029

Reference yield:

: 134217-12-2
2,6-dibromo-9-(3-O-acetyl-5-O-benzoyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-9H-purine

: 134217-13-3
2-bromo-9-(2-deoxy-2-fluoro-β-D-arabinofuranosyl)-9H-purin-6-amine

: 2-bromo-9-(5-O-benzoyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-9H-purin-6-amine

Guidance literature:: With ammonia; In ethanol; for 72h; Title compound not separated from byproducts; Ambient temperature;
DOI:10.1021/jm00080a029