2-[13-cyclohexyl-3-methoxy-10-[[[(1-methylethyl)sulfonyl]amino]carbonyl]-7H-indolo[2,1-a][2]benzazepin-6-yl]-3-furancarboxylic acid ethyl ester

Base Information

• Chemical Name: 2-[13-cyclohexyl-3-methoxy-10-[[[(1-methylethyl)sulfonyl]amino]carbonyl]-7H-indolo[2,1-a][2]benzazepin-6-yl]-3-furancarboxylic acid ethyl ester
• CAS No.: 1127238-48-5
• Molecular Formula: C₃₅H₃₈N₂O₇S
• Molecular Weight: 630.762

Synonyms:2-[13-cyclohexyl-3-methoxy-10-[[[(1-methylethyl)sulfonyl]amino]carbonyl]-7H-indolo[2,1-a][2]benzazepin-6-yl]-3-furancarboxylic acid ethyl ester

Chemical Property of 2-[13-cyclohexyl-3-methoxy-10-[[[(1-methylethyl)sulfonyl]amino]carbonyl]-7H-indolo[2,1-a][2]benzazepin-6-yl]-3-furancarboxylic acid ethyl ester

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Technology Process of 2-[13-cyclohexyl-3-methoxy-10-[[[(1-methylethyl)sulfonyl]amino]carbonyl]-7H-indolo[2,1-a][2]benzazepin-6-yl]-3-furancarboxylic acid ethyl ester

There total 1 articles about 2-[13-cyclohexyl-3-methoxy-10-[[[(1-methylethyl)sulfonyl]amino]carbonyl]-7H-indolo[2,1-a][2]benzazepin-6-yl]-3-furancarboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

1,2-dibromoethyl acetate (24442-57-7) + 13-cyclohexyl-3-methoxy-10-[[[(1-methylethyl)sulfonyl]amino]carbonyl]-beta-oxo-7H-indolo[2,1-a][2]benzazepine-6-propanoic acid ethyl ester (1127238-35-0) → 2-[13-cyclohexyl-3-methoxy-10-[[[(1-methylethyl)sulfonyl]amino]carbonyl]-7H-indolo[2,1-a][2]benzazepin-6-yl]-3-furancarboxylic acid ethyl ester (1127238-48-5) + 2-[13-cyclohexyl-3-methoxy-10-[[[(1-methylethyl)sulfonyl]amino]carbonyl]-7H-indolo[2,1-a][2]benzazepin-6-yl]-1H-pyrrole-3-carboxylic acid ethyl ester (1127238-49-6)

Guidance literature:

With ammonia; In tetrahydrofuran; at 60 ℃; under 760.051 Torr;

Reference yield: 80.0%

2-[13-cyclohexyl-3-methoxy-10-[[[(1-methylethyl)sulfonyl]amino]carbonyl]-7H-indolo[2,1-a][2]benzazepin-6-yl]-3-furancarboxylic acid ethyl ester (1127238-48-5) → 2-[13-cyclohexyl-3-methoxy-10-[[[(1-methylethyl)sulfonyl]amino]carbonyl]-7H-indolo[2,1-a][2]benzazepin-6-yl]-3-furancarboxylic acid (1127238-51-0)

Guidance literature:

With potassium trimethylsilonate; In tetrahydrofuran; at 20 ℃; for 2h;

upstream raw materials:

1,2-dibromoethyl acetate

13-cyclohexyl-3-methoxy-10-[[[(1-methylethyl)sulfonyl]amino]carbonyl]-beta-oxo-7H-indolo[2,1-a][2]benzazepine-6-propanoic acid ethyl ester

Downstream raw materials:

2-[13-cyclohexyl-3-methoxy-10-[[[(1-methylethyl)sulfonyl]amino]carbonyl]-7H-indolo[2,1-a][2]benzazepin-6-yl]-3-furancarboxylic acid

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