13-cyclohexyl-3-methoxy-10-[[[(1-methylethyl)sulfonyl]amino]carbonyl]-beta-oxo-7H-indolo[2,1-a][2]benzazepine-6-propanoic acid ethyl ester

Base Information

Chemical Name:13-cyclohexyl-3-methoxy-10-[[[(1-methylethyl)sulfonyl]amino]carbonyl]-beta-oxo-7H-indolo[2,1-a][2]benzazepine-6-propanoic acid ethyl ester
CAS No.:1127238-35-0
Molecular Formula:C₃₃H₃₈N₂O₇S
Molecular Weight:606.74
Hs Code.:

Synonyms:13-cyclohexyl-3-methoxy-10-[[[(1-methylethyl)sulfonyl]amino]carbonyl]-beta-oxo-7H-indolo[2,1-a][2]benzazepine-6-propanoic acid ethyl ester

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Chemical Property of 13-cyclohexyl-3-methoxy-10-[[[(1-methylethyl)sulfonyl]amino]carbonyl]-beta-oxo-7H-indolo[2,1-a][2]benzazepine-6-propanoic acid ethyl ester

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Technology Process of 13-cyclohexyl-3-methoxy-10-[[[(1-methylethyl)sulfonyl]amino]carbonyl]-beta-oxo-7H-indolo[2,1-a][2]benzazepine-6-propanoic acid ethyl ester

There total 1 articles about 13-cyclohexyl-3-methoxy-10-[[[(1-methylethyl)sulfonyl]amino]carbonyl]-beta-oxo-7H-indolo[2,1-a][2]benzazepine-6-propanoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1127238-38-3
13-cyclohexyl-3-methoxy-10-[[[(1-methylethyl)sulfonyl]amino]carbonyl]-7H-indolo[2,1-a][2]benzazepine-6-carboxylic acid

: 6148-64-7
ethyl potassium malonate

: 1127238-35-0
13-cyclohexyl-3-methoxy-10-[[[(1-methylethyl)sulfonyl]amino]carbonyl]-beta-oxo-7H-indolo[2,1-a][2]benzazepine-6-propanoic acid ethyl ester

Guidance literature:: 13-cyclohexyl-3-methoxy-10-[[[(1-methylethyl)sulfonyl]amino]carbonyl]-7H-indolo[2,1-a][2]benzazepine-6-carboxylic acid; With 1,1'-carbonyldiimidazole; In tetrahydrofuran; at 45 ℃; for 0.5h;

ethyl potassium malonate; With magnesium chloride; In tetrahydrofuran; at 20 - 60 ℃;

Reference yield: 35.0%

: 24442-57-7
1,2-dibromoethyl acetate

: 1127238-35-0
13-cyclohexyl-3-methoxy-10-[[[(1-methylethyl)sulfonyl]amino]carbonyl]-beta-oxo-7H-indolo[2,1-a][2]benzazepine-6-propanoic acid ethyl ester

: 75-31-0
isopropylamine

: 1127238-39-4
2-[13-cyclohexyl-3-methoxy-10-[[[(1-methylethyl)sulfonyl]amino]carbonyl]-7H-indolo[2,1-a][2]benzazepin-6-yl]-1-(1-methylethyl)-1H-pyrrole-3-carboxylic acid ethyl ester

Guidance literature:: 13-cyclohexyl-3-methoxy-10-[[[(1-methylethyl)sulfonyl]amino]carbonyl]-beta-oxo-7H-indolo[2,1-a][2]benzazepine-6-propanoic acid ethyl ester; isopropylamine; With toluene-4-sulfonic acid; In tetrahydrofuran; at 20 ℃; for 0.5h;

1,2-dibromoethyl acetate; In tetrahydrofuran; at 0 - 20 ℃; for 0.5h;

With sodium hydride; In tetrahydrofuran; at 20 - 60 ℃; for 3.16667h;