[(triphenylphosphino)aurio]acetylcymanthrene

Base Information

Chemical Name:[(triphenylphosphino)aurio]acetylcymanthrene
CAS No.:96946-12-2
Molecular Formula:C₂₈H₂₁AuMnO₄P
Molecular Weight:704.351
Hs Code.:

Synonyms:[(triphenylphosphino)aurio]acetylcymanthrene

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Chemical Property of [(triphenylphosphino)aurio]acetylcymanthrene

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Technology Process of [(triphenylphosphino)aurio]acetylcymanthrene

There total 1 articles about [(triphenylphosphino)aurio]acetylcymanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: (acetylcyclopentadienyl)tricarbonylmanganese

: 53317-87-6
tris[triphenylphosphinegold(I)]oxonium tetrafluoroborate

: 7646-69-7
sodium hydride

: 96946-12-2
[(triphenylphosphino)aurio]acetylcymanthrene

Guidance literature:: In tetrahydrofuran; mixt. stirred at room temp. for 2 h, filtration (paper filter), solventremoval (vac.), residue dissolved in benzene; pptn. with petroleum ether; elem. anal.;

Reference yield: 95.0%

: 96946-12-2
[(triphenylphosphino)aurio]acetylcymanthrene

: 75-36-5
acetyl chloride

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: 96946-13-3
(1-acetoxyvinyl)cymanthrene

Guidance literature:: In tetrahydrofuran; acetyl chloride added to the Au-complex soln.; solvent evapd. after 12 min; Mn-complex isolated by extn. (petroleum ether), purifn. by chromy. (aluminum oxide, benzene); residue of extn. dissolved in chloroform, chromy.(aluminum oxide); elem. anal.;

Reference yield: 92.0%

: 96946-12-2
[(triphenylphosphino)aurio]acetylcymanthrene

: 917-54-4
methyllithium

: methyl(triphenylphosphine)gold(I)

: (acetylcyclopentadienyl)tricarbonylmanganese

Guidance literature:: With ammonium chloride; In diethyl ether; argon atmosphere; rapid addn. of MeLi to the suspn. of the Au-complex at -5°C, mixt. stirred for 2 h at this temp. and for 1 h at room temp.; reaction mixt. decomposed with satd. NH4Cle soln., extn. (benzene); extracts are dried (K2CO3); solvent removal, residue dissolved in benzene, filtration; unchanged educt pptd. with petroleum ether; solvent removed from mother liquor, chromy. (aluminum oxide, benzene);