10-(3,4-Dimethyl-phenyl)-3-methyl-10H-pyrimido[4,5-b]quinoline-2,4-dione

Base Information

Chemical Name:10-(3,4-Dimethyl-phenyl)-3-methyl-10H-pyrimido[4,5-b]quinoline-2,4-dione
CAS No.:76896-51-0
Molecular Formula:C₂₀H₁₇N₃O₂
Molecular Weight:331.374
Hs Code.:

Synonyms:10-(3,4-Dimethyl-phenyl)-3-methyl-10H-pyrimido[4,5-b]quinoline-2,4-dione

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Chemical Property of 10-(3,4-Dimethyl-phenyl)-3-methyl-10H-pyrimido[4,5-b]quinoline-2,4-dione

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Technology Process of 10-(3,4-Dimethyl-phenyl)-3-methyl-10H-pyrimido[4,5-b]quinoline-2,4-dione

There total 3 articles about 10-(3,4-Dimethyl-phenyl)-3-methyl-10H-pyrimido[4,5-b]quinoline-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 76896-40-7
C₃₃H₃₄N₆O₄

: 76896-51-0
10-(3,4-Dimethyl-phenyl)-3-methyl-10H-pyrimido[4,5-b]quinoline-2,4-dione

Guidance literature:: With diethylazodicarboxylate; In sulfolane; at 180 - 185 ℃; for 1h;

Reference yield:

: 100-52-7
benzaldehyde

: 76896-51-0
10-(3,4-Dimethyl-phenyl)-3-methyl-10H-pyrimido[4,5-b]quinoline-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / acetic acid / 0.5 h / Heating

2: 61 percent / diethyl azodicarboxylate / tetrahydrothiophene 1,1-dioxide / 1 h / 180 - 185 °C

With diethylazodicarboxylate; In sulfolane; acetic acid;

Reference yield:

: 59776-24-8
6-(3,4-Dimethyl-anilino)-3-methyl-2,4(1H,3H)-pyrimidindion

: 76896-51-0
10-(3,4-Dimethyl-phenyl)-3-methyl-10H-pyrimido[4,5-b]quinoline-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / acetic acid / 0.5 h / Heating

2: 61 percent / diethyl azodicarboxylate / tetrahydrothiophene 1,1-dioxide / 1 h / 180 - 185 °C

With diethylazodicarboxylate; In sulfolane; acetic acid;