1-(2,6-diisopropylphenyl)-3-[3-(trimethoxysilyl)propyl]imidazolium iodide

Base Information

• Chemical Name: 1-(2,6-diisopropylphenyl)-3-[3-(trimethoxysilyl)propyl]imidazolium iodide
• CAS No.: 1174062-53-3
• Molecular Formula: C₂₁H₃₅N₂O₃Si*I
• Molecular Weight: 518.51

Synonyms:1-(2,6-diisopropylphenyl)-3-[3-(trimethoxysilyl)propyl]imidazolium iodide

Chemical Property of 1-(2,6-diisopropylphenyl)-3-[3-(trimethoxysilyl)propyl]imidazolium iodide

Chemical Property:

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Technology Process of 1-(2,6-diisopropylphenyl)-3-[3-(trimethoxysilyl)propyl]imidazolium iodide

There total 2 articles about 1-(2,6-diisopropylphenyl)-3-[3-(trimethoxysilyl)propyl]imidazolium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

1-(2,6-diisopropylphenyl)-1H-imidazole (25364-47-0) + 3-iodopropyltrimethoxysilane (14867-28-8) → 1-(2,6-diisopropylphenyl)-3-[3-(trimethoxysilyl)propyl]imidazolium iodide (1174062-53-3)

Guidance literature:

In acetonitrile; at 100 ℃; for 7h; Inert atmosphere;

DOI:10.1016/j.jorganchem.2011.06.042

Reference yield: 64.0%

1-(2,6-diisopropylphenyl)-1H-imidazole (25364-47-0) + 3-Chloropropyltrimethoxysilan (2530-87-2) → 1-(2,6-diisopropylphenyl)-3-[3-(trimethoxysilyl)propyl]imidazolium iodide (1174062-53-3)

Guidance literature:

With potassium iodide; In 1,2-dimethoxyethane; at 85 ℃; for 47h; Inert atmosphere;

DOI:10.1055/s-0028-1088053

Reference yield:

nickelocene (1271-28-9) + 1-(2,6-diisopropylphenyl)-3-[3-(trimethoxysilyl)propyl]imidazolium iodide (1174062-53-3) → [(η5-cyclopentadienyl)NiI(1-(2,6-diisopropylphenyl)-3-[3-(trimethoxysilyl)propyl]imidazol-2-ylidene)]

Guidance literature:

In 1,2-dimethoxyethane; (Ar); refluxing nickelocene and imidazolium deriv. in DME;

DOI:10.1021/om201101g

upstream raw materials:

1-(2,6-diisopropylphenyl)-1H-imidazole

3-Chloropropyltrimethoxysilan

3-iodopropyltrimethoxysilane

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