N-Boc-glycyl-L-prolyl-glycyl-L-prolyl-S-trityl-L-cysteine benzhydryl ester

Base Information

Chemical Name:N-Boc-glycyl-L-prolyl-glycyl-L-prolyl-S-trityl-L-cysteine benzhydryl ester
CAS No.:118002-58-7
Molecular Formula:C₅₄H₅₉N₅O₈S
Molecular Weight:938.157
Hs Code.:

Synonyms:N-Boc-glycyl-L-prolyl-glycyl-L-prolyl-S-trityl-L-cysteine benzhydryl ester

Suppliers and Price of N-Boc-glycyl-L-prolyl-glycyl-L-prolyl-S-trityl-L-cysteine benzhydryl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Boc-glycyl-L-prolyl-glycyl-L-prolyl-S-trityl-L-cysteine benzhydryl ester

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Technology Process of N-Boc-glycyl-L-prolyl-glycyl-L-prolyl-S-trityl-L-cysteine benzhydryl ester

There total 9 articles about N-Boc-glycyl-L-prolyl-glycyl-L-prolyl-S-trityl-L-cysteine benzhydryl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16652-71-4
benzyl (2S)-2-pyrrolidinecarboxylate hydrochloride

: 118002-58-7
N-Boc-glycyl-L-prolyl-glycyl-L-prolyl-S-trityl-L-cysteine benzhydryl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) EEDQ; 2.) triethylamine / 1.) EEDQ, methylene chloride, 5 min; 2.) triethylamine, methylene chloride, RT, 20 h

2: 98 percent / H₂ / 10percent Pd on carbon / methanol / 4 h / atmospheric pressure

3: 1.) EEDQ; 2.) triethylamine / 1.) EEDQ, methylene chloride, RT, 5 min; 2.) triethylamine, RT, 20 h

4: 93 percent / H₂ / 10percent Pd on carbon / methanol / 5 h / atmospheric pressure

5: 1.) EEDQ; 2.) triethylamine / 1.) EEDQ, methanol, 5 min; 2.) triethylamine, 44 h

With hydrogen; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; triethylamine; palladium on activated charcoal; In methanol;
DOI:10.1139/v88-425

Reference yield:

: 4530-20-5
BOC-glycine

: 118002-58-7
N-Boc-glycyl-L-prolyl-glycyl-L-prolyl-S-trityl-L-cysteine benzhydryl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) EEDQ; 2.) triethylamine / 1.) EEDQ, methylene chloride, 5 min; 2.) triethylamine, methylene chloride, RT, 20 h

2: 98 percent / H₂ / 10percent Pd on carbon / methanol / 4 h / atmospheric pressure

3: 1.) EEDQ; 2.) triethylamine / 1.) EEDQ, methylene chloride, RT, 5 min; 2.) triethylamine, RT, 20 h

4: 93 percent / H₂ / 10percent Pd on carbon / methanol / 5 h / atmospheric pressure

5: 1.) EEDQ; 2.) triethylamine / 1.) EEDQ, methanol, 5 min; 2.) triethylamine, 44 h

With hydrogen; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; triethylamine; palladium on activated charcoal; In methanol;
DOI:10.1139/v88-425

Reference yield:

: 14296-92-5
(S)-1-(2-(tert-butoxycarbonylamino)acetyl)pyrrolidine-2-carboxylic acid

: 118002-58-7
N-Boc-glycyl-L-prolyl-glycyl-L-prolyl-S-trityl-L-cysteine benzhydryl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) EEDQ; 2.) triethylamine / 1.) EEDQ, methylene chloride, RT, 5 min; 2.) triethylamine, RT, 20 h

2: 93 percent / H₂ / 10percent Pd on carbon / methanol / 5 h / atmospheric pressure

3: 1.) EEDQ; 2.) triethylamine / 1.) EEDQ, methanol, 5 min; 2.) triethylamine, 44 h

With hydrogen; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; triethylamine; palladium on activated charcoal; In methanol;
DOI:10.1139/v88-425