diisopropyl (3-(6-fluorobenzo[d]thiazol-2-yl)thioureido)(phenyl)methylphosphonate

Base Information

Chemical Name:diisopropyl (3-(6-fluorobenzo[d]thiazol-2-yl)thioureido)(phenyl)methylphosphonate
CAS No.:1352612-48-6
Molecular Formula:C₂₁H₂₅FN₃O₃PS₂
Molecular Weight:481.552
Hs Code.:

Synonyms:diisopropyl (3-(6-fluorobenzo[d]thiazol-2-yl)thioureido)(phenyl)methylphosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diisopropyl (3-(6-fluorobenzo[d]thiazol-2-yl)thioureido)(phenyl)methylphosphonate

Chemical Property:

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Technology Process of diisopropyl (3-(6-fluorobenzo[d]thiazol-2-yl)thioureido)(phenyl)methylphosphonate

There total 5 articles about diisopropyl (3-(6-fluorobenzo[d]thiazol-2-yl)thioureido)(phenyl)methylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.2%

: 348-40-3
2-amino-6-fluoro-1,3-benzothiazole

: 1192761-59-3
O,O'-diisopropyl isothiocyanato(phenyl)methylphosphonate

: 1352612-48-6
diisopropyl (3-(6-fluorobenzo[d]thiazol-2-yl)thioureido)(phenyl)methylphosphonate

Guidance literature:: In acetonitrile; at 90 ℃; for 0.5h; Microwave irradiation;
DOI:10.1080/10426507.2011.575422

Reference yield:

: O,O-diisopropyl (benzylideneamino)(phenyl)methanephosphonate

: 1352612-48-6
diisopropyl (3-(6-fluorobenzo[d]thiazol-2-yl)thioureido)(phenyl)methylphosphonate

Guidance literature:: Multi-step reaction with 4 steps

1: water

2: ammonium hydroxide

3: bis(trichloromethyl) carbonate; triethylamine / diethyl ether

4: acetonitrile / 0.5 h / 90 °C / Microwave irradiation

With ammonium hydroxide; bis(trichloromethyl) carbonate; triethylamine; In diethyl ether; water; acetonitrile;
DOI:10.1080/10426507.2011.575422

Reference yield:

: 1038997-71-5
C₇H₈O₃S*C₁₃H₂₂NO₃P

: 1352612-48-6
diisopropyl (3-(6-fluorobenzo[d]thiazol-2-yl)thioureido)(phenyl)methylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium hydroxide

2: bis(trichloromethyl) carbonate; triethylamine / diethyl ether

3: acetonitrile / 0.5 h / 90 °C / Microwave irradiation

With ammonium hydroxide; bis(trichloromethyl) carbonate; triethylamine; In diethyl ether; acetonitrile;
DOI:10.1080/10426507.2011.575422