10-{4-[3-(benzoyloxy)propyloxy]benzoylmethyl}-1,4,7,10-tetraazacyclododecane-1,4,7-triacetic acid tris(1,1-dimethylethyl) ester

Base Information

Chemical Name:10-{4-[3-(benzoyloxy)propyloxy]benzoylmethyl}-1,4,7,10-tetraazacyclododecane-1,4,7-triacetic acid tris(1,1-dimethylethyl) ester
CAS No.:882685-65-6
Molecular Formula:C₄₄H₆₆N₄O₁₀
Molecular Weight:811.029
Hs Code.:

Synonyms:10-{4-[3-(benzoyloxy)propyloxy]benzoylmethyl}-1,4,7,10-tetraazacyclododecane-1,4,7-triacetic acid tris(1,1-dimethylethyl) ester

Suppliers and Price of 10-{4-[3-(benzoyloxy)propyloxy]benzoylmethyl}-1,4,7,10-tetraazacyclododecane-1,4,7-triacetic acid tris(1,1-dimethylethyl) ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 10-{4-[3-(benzoyloxy)propyloxy]benzoylmethyl}-1,4,7,10-tetraazacyclododecane-1,4,7-triacetic acid tris(1,1-dimethylethyl) ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 10-{4-[3-(benzoyloxy)propyloxy]benzoylmethyl}-1,4,7,10-tetraazacyclododecane-1,4,7-triacetic acid tris(1,1-dimethylethyl) ester

There total 3 articles about 10-{4-[3-(benzoyloxy)propyloxy]benzoylmethyl}-1,4,7,10-tetraazacyclododecane-1,4,7-triacetic acid tris(1,1-dimethylethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-(4-acetylphenoxy)propyl benzoate

: 882685-65-6
10-{4-[3-(benzoyloxy)propyloxy]benzoylmethyl}-1,4,7,10-tetraazacyclododecane-1,4,7-triacetic acid tris(1,1-dimethylethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / N-bromosuccinimide; p-TsOH*H₂O / acetonitrile / 1 h / Heating

2: 91 percent / Na₂CO₃ / acetonitrile / 30 h / Heating

With N-Bromosuccinimide; sodium carbonate; toluene-4-sulfonic acid; In acetonitrile;
DOI:10.1039/b514409d

Reference yield:

: 6065-69-6
3-bromopropyl benzoate

: 882685-65-6
10-{4-[3-(benzoyloxy)propyloxy]benzoylmethyl}-1,4,7,10-tetraazacyclododecane-1,4,7-triacetic acid tris(1,1-dimethylethyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / Na₂CO₃ / acetonitrile / 120 h / Heating

2: 83 percent / N-bromosuccinimide; p-TsOH*H₂O / acetonitrile / 1 h / Heating

3: 91 percent / Na₂CO₃ / acetonitrile / 30 h / Heating

With N-Bromosuccinimide; sodium carbonate; toluene-4-sulfonic acid; In acetonitrile;
DOI:10.1039/b514409d

Reference yield:

: 99-93-4
4-Hydroxyacetophenone

: 882685-65-6
10-{4-[3-(benzoyloxy)propyloxy]benzoylmethyl}-1,4,7,10-tetraazacyclododecane-1,4,7-triacetic acid tris(1,1-dimethylethyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / Na₂CO₃ / acetonitrile / 120 h / Heating

2: 83 percent / N-bromosuccinimide; p-TsOH*H₂O / acetonitrile / 1 h / Heating

3: 91 percent / Na₂CO₃ / acetonitrile / 30 h / Heating

With N-Bromosuccinimide; sodium carbonate; toluene-4-sulfonic acid; In acetonitrile;
DOI:10.1039/b514409d