3-bromopropyl benzoate

Base Information

• Chemical Name: 3-bromopropyl benzoate
• CAS No.: 6065-69-6
• Molecular Formula: C₁₀H₁₁BrO₂
• Molecular Weight: 243.1

Synonyms:3-bromopropyl benzoate

Chemical Property of 3-bromopropyl benzoate

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-bromopropyl benzoate

There total 7 articles about 3-bromopropyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

benzoyl chloride (98-88-4) + 1-bromo-3-propanol (627-18-9) → 3-bromopropyl benzoate (6065-69-6)

Guidance literature:

With triethylamine; In diethyl ether; at 0 - 20 ℃; for 9.5h;

DOI:10.1021/jo061880o

Reference yield: 89.0%

2-phenyl-1,3-dioxane (772-01-0) → 3-bromopropyl benzoate (6065-69-6)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); Bromoform; In benzene; for 5h; Heating;

DOI:10.1080/00397919708005032

Reference yield: 80.0%

1-benzoylimidazole (10364-94-0) + 1-bromo-3-propanol (627-18-9) → 3-bromopropyl benzoate (6065-69-6)

Guidance literature:

With pyridinium p-toluenesulfonate; In acetonitrile; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1021/ol300339q

upstream raw materials:

sodium benzoate

1,3-dibromo-propane

2-phenyl-1,3-dioxane

benzaldehyde

Downstream raw materials:

benzoic acid (3-iodopropyl) ester

1-benzoyloxy-3-diethylamino-propane

3-hydroxy-N-phenylpropylamine

1-benzoyloxy-3-methylamino-propane

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