(S,S)-N-BENZYL-3,4-TRANS-(N-BOC)-DIAMINOPYRROLIDINE

Base Information

Chemical Name:(S,S)-N-BENZYL-3,4-TRANS-(N-BOC)-DIAMINOPYRROLIDINE
CAS No.:266692-94-8
Molecular Formula:C21H33 N3 O4
Molecular Weight:359.51
Hs Code.:
Mol file:266692-94-8.mol

Synonyms:(S,S)-N-BENZYL-3,4-TRANS-(N-BOC)-DIAMINOPYRROLIDINE

Suppliers and Price of (S,S)-N-BENZYL-3,4-TRANS-(N-BOC)-DIAMINOPYRROLIDINE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(S,S)-N-BENZYL-3,4-TRANS-(N-BOC)- DIAMINOPYRROLIDINE 95.00%
100MG
$ 595.35

American Custom Chemicals Corporation
(S,S)-N-BENZYL-3,4-TRANS-(N-BOC)- DIAMINOPYRROLIDINE 95.00%
5MG
$ 495.23

Total 6 raw suppliers

Chemical Property of (S,S)-N-BENZYL-3,4-TRANS-(N-BOC)-DIAMINOPYRROLIDINE

Chemical Property:

PSA：61.44000
LogP:3.28370

Purity/Quality:

97% ^*data from raw suppliers

(S,S)-N-BENZYL-3,4-TRANS-(N-BOC)- DIAMINOPYRROLIDINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (S,S)-N-BENZYL-3,4-TRANS-(N-BOC)-DIAMINOPYRROLIDINE

There total 5 articles about (S,S)-N-BENZYL-3,4-TRANS-(N-BOC)-DIAMINOPYRROLIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 193352-75-9,246149-02-0
(3S,4S)-1-benzyl-pyrrolidine-3,4-diamine

: 266692-94-8
N-benzyl-3,4-di(Boc-amino)pyrrolidine

Guidance literature:: In dichloromethane; Ambient temperature;
DOI:10.1016/S0960-894X(98)00063-8

Reference yield:

: 163439-82-5,330152-66-4
(3R,4R)-1-benzyl-3,4-pyrrolidinediol

: 266692-94-8
N-benzyl-3,4-di(Boc-amino)pyrrolidine

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / HN₃; DEAD; PPh₃

2: LiAlH₄ / tetrahydrofuran / 0.5 h / Heating

3: 1.5 g / NaOH / H₂O; dioxane / 2 h / 20 °C

With sodium hydroxide; lithium aluminium tetrahydride; tris-(2-chloro-ethyl)-amine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 1,4-dioxane; water; 1: Substitution / 2: Reduction / 3: Substitution;
DOI:10.1021/jo991628z

Reference yield:

: 187032-53-7
(3S,4S)-1-N-benzyl-3,4-dihydroxypyrrolidine-2,6-dione

: 266692-94-8
N-benzyl-3,4-di(Boc-amino)pyrrolidine

Guidance literature:: Multi-step reaction with 4 steps

1: 67 percent / NaBH₄; BF₃*Et₂O

2: 95 percent / HN₃; DEAD; PPh₃

3: LiAlH₄ / tetrahydrofuran / 0.5 h / Heating

4: 1.5 g / NaOH / H₂O; dioxane / 2 h / 20 °C

With sodium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; tris-(2-chloro-ethyl)-amine; boron trifluoride diethyl etherate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 1,4-dioxane; water; 1: Reduction / 2: Substitution / 3: Reduction / 4: Substitution;
DOI:10.1021/jo991628z