(R)-N-methoxy-N-methyl-2-(4-nitrophenyl)-4,5-dihydrothiazole-4-carboxamide

Base Information

Chemical Name:(R)-N-methoxy-N-methyl-2-(4-nitrophenyl)-4,5-dihydrothiazole-4-carboxamide
CAS No.:1135797-75-9
Molecular Formula:C₁₂H₁₃N₃O₄S
Molecular Weight:295.319
Hs Code.:

Synonyms:(R)-N-methoxy-N-methyl-2-(4-nitrophenyl)-4,5-dihydrothiazole-4-carboxamide

Suppliers and Price of (R)-N-methoxy-N-methyl-2-(4-nitrophenyl)-4,5-dihydrothiazole-4-carboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-N-methoxy-N-methyl-2-(4-nitrophenyl)-4,5-dihydrothiazole-4-carboxamide

Chemical Property:

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Technology Process of (R)-N-methoxy-N-methyl-2-(4-nitrophenyl)-4,5-dihydrothiazole-4-carboxamide

There total 1 articles about (R)-N-methoxy-N-methyl-2-(4-nitrophenyl)-4,5-dihydrothiazole-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.7%

: 1196463-60-1
(R)-2-(4-nitrophenyl)-4,5-dihydrothiazole-4-carboxylic acid

: 1117-97-1
N,0-dimethylhydroxylamine

: 1135797-75-9
(R)-N-methoxy-N-methyl-2-(4-nitrophenyl)-4,5-dihydrothiazole-4-carboxamide

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;
DOI:10.1021/jm801449a

Reference yield:

: 1135797-75-9
(R)-N-methoxy-N-methyl-2-(4-nitrophenyl)-4,5-dihydrothiazole-4-carboxamide

: 1202516-96-8
C₁₂H₁₁N₃O₄S

Guidance literature:: With Bromotrichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jm801449a

Reference yield:

: 1135797-75-9
(R)-N-methoxy-N-methyl-2-(4-nitrophenyl)-4,5-dihydrothiazole-4-carboxamide

: 2675-79-8
1-bromo-3,4,5-trimethoxybenzene

: 1135798-04-7
[2-(4-nitrophenyl)thiazol-4-yl](3,4,5-trimethoxyphenyl)methanone

Guidance literature:: 1-bromo-3,4,5-trimethoxybenzene; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 2h; Inert atmosphere;

(R)-N-methoxy-N-methyl-2-(4-nitrophenyl)-4,5-dihydrothiazole-4-carboxamide; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;

With air; In diethyl ether; at 20 ℃;
DOI:10.1021/jm801449a