Phosphoric acid 2-benzenesulfonyl-ethyl ester 2-chloro-phenyl ester (2R,3S,5R)-2-hydroxymethyl-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

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Chemical Name:Phosphoric acid 2-benzenesulfonyl-ethyl ester 2-chloro-phenyl ester (2R,3S,5R)-2-hydroxymethyl-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester
CAS No.:79258-45-0
Molecular Formula:C₂₄H₂₆ClN₂O₁₀PS
Molecular Weight:600.971
Hs Code.:

Phosphoric acid 2-benzenesulfonyl-ethyl ester 2-chloro-phenyl ester (2R,3S,5R)-2-hydroxymethyl-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

Synonyms:Phosphoric acid 2-benzenesulfonyl-ethyl ester 2-chloro-phenyl ester (2R,3S,5R)-2-hydroxymethyl-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

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Chemical Property of Phosphoric acid 2-benzenesulfonyl-ethyl ester 2-chloro-phenyl ester (2R,3S,5R)-2-hydroxymethyl-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

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Technology Process of Phosphoric acid 2-benzenesulfonyl-ethyl ester 2-chloro-phenyl ester (2R,3S,5R)-2-hydroxymethyl-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

There total 1 articles about Phosphoric acid 2-benzenesulfonyl-ethyl ester 2-chloro-phenyl ester (2R,3S,5R)-2-hydroxymethyl-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2-Benzenesulfonyl-ethyl)-phosphonic acid 2-chloro-phenyl ester (2R,3S,5R)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-(9-phenyl-9H-xanthen-9-yloxymethyl)-tetrahydro-furan-3-yl ester

: 79258-45-0
Phosphoric acid 2-benzenesulfonyl-ethyl ester 2-chloro-phenyl ester (2R,3S,5R)-2-hydroxymethyl-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

Guidance literature:: With water; toluene-4-sulfonic acid; In ethanol; chloroform;
DOI:10.1016/S0040-4039(01)90477-0

Reference yield: 83.0%

: 79258-45-0
Phosphoric acid 2-benzenesulfonyl-ethyl ester 2-chloro-phenyl ester (2R,3S,5R)-2-hydroxymethyl-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

: 79258-44-9
5'-O-(9-phenylxanthen-9-yl)thymidine-3'-(2-chlorophenyl) phosphate

: 79258-42-7
C₅₉H₅₄Cl₂N₄O₁₈P₂S

Guidance literature:: With 1-(mesitylene-2-sulfonyl)-3-nitro-1H-1,2,4-triazole; In pyridine;
DOI:10.1016/S0040-4039(01)90477-0

Reference yield:

: 79258-45-0
Phosphoric acid 2-benzenesulfonyl-ethyl ester 2-chloro-phenyl ester (2R,3S,5R)-2-hydroxymethyl-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

: 79275-85-7
C₅₁H₄₆Cl₂N₄O₁₆P₂*C₆H₁₅N

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / 1-mesitylenesulfonyl-3-nitro-1,2,4-triazole / pyridine

2: pyridine / 3 h / 20 °C

With 1-(mesitylene-2-sulfonyl)-3-nitro-1H-1,2,4-triazole; In pyridine;
DOI:10.1016/S0040-4039(01)90477-0