(C₅H₅)Fe(C(NHCH₃)CH₃)(CO)(P(C₆H₅)3)⁽¹⁺⁾*BF₄^(1-) = [(C₅H₅)Fe(C(NHCH₃)CH₃)(CO)(P(C₆H₅)3)]BF₄

Base Information

• Chemical Name: (C₅H₅)Fe(C(NHCH₃)CH₃)(CO)(P(C₆H₅)3)⁽¹⁺⁾*BF₄^(1-) = [(C₅H₅)Fe(C(NHCH₃)CH₃)(CO)(P(C₆H₅)3)]BF₄
• CAS No.: 80662-48-2
• Molecular Formula: BF₄*C₂₇H₂₇FeNOP
• Molecular Weight: 555.143

Synonyms:(C₅H₅)Fe(C(NHCH₃)CH₃)(CO)(P(C₆H₅)3)⁽¹⁺⁾*BF₄^(1-) = [(C₅H₅)Fe(C(NHCH₃)CH₃)(CO)(P(C₆H₅)3)]BF₄

Chemical Property of (C₅H₅)Fe(C(NHCH₃)CH₃)(CO)(P(C₆H₅)3)⁽¹⁺⁾*BF₄^(1-) = [(C₅H₅)Fe(C(NHCH₃)CH₃)(CO)(P(C₆H₅)3)]BF₄

Chemical Property:

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Technology Process of (C₅H₅)Fe(C(NHCH₃)CH₃)(CO)(P(C₆H₅)3)⁽¹⁺⁾*BF₄^(1-) = [(C₅H₅)Fe(C(NHCH₃)CH₃)(CO)(P(C₆H₅)3)]BF₄

There total 2 articles about (C₅H₅)Fe(C(NHCH₃)CH₃)(CO)(P(C₆H₅)3)⁽¹⁺⁾*BF₄^(1-) = [(C₅H₅)Fe(C(NHCH₃)CH₃)(CO)(P(C₆H₅)3)]BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

(C5H5)Fe(C(OCH3)CH3)(CO)(P(C6H5)3)(1+)*BF4(1-) = [(C5H5)Fe(C(OCH3)CH3)(CO)(P(C6H5)3)]BF4 (32610-60-9) + methylamine (74-89-5) → (C5H5)Fe(C(NHCH3)CH3)(CO)(P(C6H5)3)(1+)*BF4(1-) = [(C5H5)Fe(C(NHCH3)CH3)(CO)(P(C6H5)3)]BF4 (80662-48-2)

Guidance literature:

In tetrahydrofuran; (N2); concn. (vac.), dissoln. (min. amt. CH2Cl2), pptn. upon cannulation into Et2O at 0°C, removal of solvent, washing (Et2O), drying (vac.);

DOI:10.1039/a800927i

Reference yield: 75.0%

{Cp(CO)(Ph3P)FeCCH2}BF4 → acetyl carbonyl cyclopentadienyl triphenylphosphine iron + Fe(C5H5)(CO)P(C6H5)3CCH (80642-59-7) + (C5H5)Fe(C(NHCH3)CH3)(CO)(P(C6H5)3)(1+)*BF4(1-) = [(C5H5)Fe(C(NHCH3)CH3)(CO)(P(C6H5)3)]BF4 (80662-48-2)

Guidance literature:

With methylamine; In neat (no solvent); MeNH2 was condensed on to complex at -196°C, the mixt. was warmed to -24°C and stirred for 1 h (N2 atm.);; evapd., chromd. in silica gel column with Et2O-CH2Cl2; recrystd.;

Reference yield: 96.0%

ammonium hexafluorophosphate + (C5H5)Fe(C(NHCH3)CH3)(CO)(P(C6H5)3)(1+)*BF4(1-) = [(C5H5)Fe(C(NHCH3)CH3)(CO)(P(C6H5)3)]BF4 (80662-48-2) → (C5H5)Fe(C(NHCH3)CH3)(CO)(P(C6H5)3)(1+)*PF6(1-) = [(C5H5)Fe(C(NHCH3)CH3)(CO)(P(C6H5)3)]PF6

Guidance literature:

In water; acetone; (N2); addn. of satd. aq. NH4PF6 to the Fe complex in acetone at room temp.; filtration, washing (H2O; EtOH; Et2O), recrystn. (CH2Cl2/Et2O); elem. anal.;

DOI:10.1039/a800927i

upstream raw materials:

(C₅H₅)Fe(C(OCH₃)CH₃)(CO)(P(C₆H₅)3)⁽¹⁺⁾*BF₄^(1-) = [(C₅H₅)Fe(C(OCH₃)CH₃)(CO)(P(C₆H₅)3)]BF₄

methylamine

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