1-(2,5-dichlorophenyl)ethylidenethiosemicarbazone

Base Information

Chemical Name:1-(2,5-dichlorophenyl)ethylidenethiosemicarbazone
CAS No.:18087-40-6
Molecular Formula:C₉H₉Cl₂N₃S
Molecular Weight:262.163
Hs Code.:

Synonyms:1-(2,5-dichlorophenyl)ethylidenethiosemicarbazone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2,5-dichlorophenyl)ethylidenethiosemicarbazone

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Technology Process of 1-(2,5-dichlorophenyl)ethylidenethiosemicarbazone

There total 1 articles about 1-(2,5-dichlorophenyl)ethylidenethiosemicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 2476-37-1
2,5-dichloroacetophenone

: 79-19-6
thiosemicarbazide

: 18087-40-6
1-(2,5-dichlorophenyl)ethylidenethiosemicarbazone

Guidance literature:: With sulfuric acid; In ethanol; for 2h; Irradiation;
DOI:10.1016/j.cbi.2021.109514

Reference yield: 87.0%

: 18087-40-6
1-(2,5-dichlorophenyl)ethylidenethiosemicarbazone

: 533-68-6
2-bromobutyric acid ethyl ester

: 2-[1-(2,5-dichlorophenyl)ethylidenohydrazone]-5-ethylthiazolidin-4-one

Guidance literature:: 1-(2,5-dichlorophenyl)ethylidenethiosemicarbazone; With sodium acetate; In ethanol; for 0.25h;

2-bromobutyric acid ethyl ester; In ethanol; for 24h; Reflux;
DOI:10.1016/j.cbi.2021.109514

Reference yield: 70.0%

: 18087-40-6
1-(2,5-dichlorophenyl)ethylidenethiosemicarbazone

: 105-36-2
ethyl bromoacetate

: 2-[1-(2,5-dichlorophenyl)ethylidenohydrazone]thiazolidin-4-one

Guidance literature:: 1-(2,5-dichlorophenyl)ethylidenethiosemicarbazone; With sodium acetate; In ethanol; for 0.25h;

ethyl bromoacetate; In ethanol; for 24h; Reflux;
DOI:10.1016/j.cbi.2021.109514