C₇H₇BrClN

Base Information

• Chemical Name: C₇H₇BrClN
• CAS No.: 1003859-10-6
• Molecular Formula: C₇H₇BrClN
• Molecular Weight: 220.496
• Mol file: 1003859-10-6.mol

Synonyms:C₇H₇BrClN

Chemical Property of C₇H₇BrClN

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

5-(Bromomethyl)-2-chloro-3-methylpyridine 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₇H₇BrClN

There total 3 articles about C₇H₇BrClN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-bromo-2-chloro-3-methylpyridine (29241-60-9) → C7H7BrClN (1003859-10-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran / 2 h / -78 °C

1.2: 0.5 h

2.1: triphenylphosphine; carbon tetrabromide / dichloromethane / 0.5 h / 20 °C

With n-butyllithium; carbon tetrabromide; triphenylphosphine; In tetrahydrofuran; dichloromethane;

Reference yield:

(6-chloro-5-methylpyridin-3-yl)methanol (887707-21-3) → C7H7BrClN (1003859-10-6)

Guidance literature:

With carbon tetrabromide; triphenylphosphine; In dichloromethane; at 20 ℃; for 0.5h;

Reference yield:

→ C7H7BrClN (1003859-10-6)

Guidance literature:

upstream raw materials:

5-bromo-2-chloro-3-methylpyridine

(6-chloro-5-methylpyridin-3-yl)methanol

Refernces

• 1、 -. "N'-Cyano-N-Halogenalkylimidamide Derivatives". Page/Page column 25-26. . Retrieved 2010/03/31.
• 2、 -. "SUBSTITUTED ENAMINOCARBONYL COMPOUNDS". Page/Page column 28. . Retrieved 2009/10/06.