4-methoxyphenyl 2-O-acetyl-4-O-benzyl-3-O-(fluorenylmethoxycarbonyl)-α-L-rhamnopyranoside

Base Information

Chemical Name:4-methoxyphenyl 2-O-acetyl-4-O-benzyl-3-O-(fluorenylmethoxycarbonyl)-α-L-rhamnopyranoside
CAS No.:870543-49-0
Molecular Formula:C₃₇H₃₆O₉
Molecular Weight:624.687
Hs Code.:

Synonyms:4-methoxyphenyl 2-O-acetyl-4-O-benzyl-3-O-(fluorenylmethoxycarbonyl)-α-L-rhamnopyranoside

Suppliers and Price of 4-methoxyphenyl 2-O-acetyl-4-O-benzyl-3-O-(fluorenylmethoxycarbonyl)-α-L-rhamnopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methoxyphenyl 2-O-acetyl-4-O-benzyl-3-O-(fluorenylmethoxycarbonyl)-α-L-rhamnopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 4-methoxyphenyl 2-O-acetyl-4-O-benzyl-3-O-(fluorenylmethoxycarbonyl)-α-L-rhamnopyranoside

There total 1 articles about 4-methoxyphenyl 2-O-acetyl-4-O-benzyl-3-O-(fluorenylmethoxycarbonyl)-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 870543-37-6
p-methoxyphenyl 2-O-acetyl-4-O-benzyl-α-L-rhamnopyranoside

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 870543-49-0
4-methoxyphenyl 2-O-acetyl-4-O-benzyl-3-O-(fluorenylmethoxycarbonyl)-α-L-rhamnopyranoside

Guidance literature:: With pyridine; at 25 ℃; for 2h;
DOI:10.1002/anie.200502615

Reference yield: 76.0%

: 870543-49-0
4-methoxyphenyl 2-O-acetyl-4-O-benzyl-3-O-(fluorenylmethoxycarbonyl)-α-L-rhamnopyranoside

: 870543-48-9
2-acetyl-4-benzyl-3-fluorenylmethoxycarbonyl-L-rhamnopyranoside

Guidance literature:: With ammonium cerium(IV) nitrate; In water; toluene; acetonitrile; at 25 ℃; for 1.33333h;

Reference yield:

: 870543-49-0
4-methoxyphenyl 2-O-acetyl-4-O-benzyl-3-O-(fluorenylmethoxycarbonyl)-α-L-rhamnopyranoside

: 870543-38-7
2-O-acetyl-4-O-benzyl-3-O-(fluorenylmethoxycarbonyl)-α-L-rhamnopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / cerium(IV) ammonium nitrate / acetonitrile; H₂O; toluene / 1.33 h / 20 °C

2: 94 percent / sodium hydride / CH₂Cl₂ / 1 h / 25 °C

With ammonium cerium(IV) nitrate; sodium hydride; In dichloromethane; water; toluene; acetonitrile;
DOI:10.1002/anie.200502615