(1R,1'R)-2-[N-(2,4,6-trimethoxybenzyl)-N-2'-hydroxy-1'-phenylethylamino]-5,5-ethylenedioxy-1-phenylpentane

Base Information

Chemical Name:(1R,1'R)-2-[N-(2,4,6-trimethoxybenzyl)-N-2'-hydroxy-1'-phenylethylamino]-5,5-ethylenedioxy-1-phenylpentane
CAS No.:205526-53-0
Molecular Formula:C₃₁H₃₉NO₆
Molecular Weight:521.654
Hs Code.:

Synonyms:(1R,1'R)-2-[N-(2,4,6-trimethoxybenzyl)-N-2'-hydroxy-1'-phenylethylamino]-5,5-ethylenedioxy-1-phenylpentane

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Chemical Property of (1R,1'R)-2-[N-(2,4,6-trimethoxybenzyl)-N-2'-hydroxy-1'-phenylethylamino]-5,5-ethylenedioxy-1-phenylpentane

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Technology Process of (1R,1'R)-2-[N-(2,4,6-trimethoxybenzyl)-N-2'-hydroxy-1'-phenylethylamino]-5,5-ethylenedioxy-1-phenylpentane

There total 4 articles about (1R,1'R)-2-[N-(2,4,6-trimethoxybenzyl)-N-2'-hydroxy-1'-phenylethylamino]-5,5-ethylenedioxy-1-phenylpentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.4%

: 100-58-3
phenylmagnesium bromide

: 205526-52-9
(2R,4R)-2-(3-[1,3]Dioxolan-2-yl-propyl)-4-phenyl-3-(2,4,6-trimethoxy-benzyl)-oxazolidine

: 205526-53-0
(1R,1'R)-2-[N-(2,4,6-trimethoxybenzyl)-N-2'-hydroxy-1'-phenylethylamino]-5,5-ethylenedioxy-1-phenylpentane

Guidance literature:: In tetrahydrofuran; at 0 ℃; for 72h;
DOI:10.3987/com-97-s32

Reference yield:

: 830-79-5
2,4,6-trimethoxybenzaldehyde

: 205526-53-0
(1R,1'R)-2-[N-(2,4,6-trimethoxybenzyl)-N-2'-hydroxy-1'-phenylethylamino]-5,5-ethylenedioxy-1-phenylpentane

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) sodium borohydride / 1.) benzene, reflux, 1 h; 2.) MeOH, r.t., 40 min

2: 100 percent / Na₂SO₄ / CH₂Cl₂ / 48 h / Ambient temperature

3: 93.4 percent / tetrahydrofuran / 72 h / 0 °C

With sodium tetrahydroborate; sodium sulfate; In tetrahydrofuran; dichloromethane;
DOI:10.3987/com-97-s32

Reference yield:

: 56613-80-0
D-2-phenylglycinol

: 205526-53-0
(1R,1'R)-2-[N-(2,4,6-trimethoxybenzyl)-N-2'-hydroxy-1'-phenylethylamino]-5,5-ethylenedioxy-1-phenylpentane

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) sodium borohydride / 1.) benzene, reflux, 1 h; 2.) MeOH, r.t., 40 min

2: 100 percent / Na₂SO₄ / CH₂Cl₂ / 48 h / Ambient temperature

3: 93.4 percent / tetrahydrofuran / 72 h / 0 °C

With sodium tetrahydroborate; sodium sulfate; In tetrahydrofuran; dichloromethane;
DOI:10.3987/com-97-s32