C₂₉H₂₇⁽²⁾H₄O₆I

Base Information

• Chemical Name: C₂₉H₂₇⁽²⁾H₄O₆I
• CAS No.: 945033-20-5
• Molecular Formula: C₂₉H₃₁IO₆
• Molecular Weight: 606.434
• Mol file: 945033-20-5.mol

Synonyms:C₂₉H₂₇⁽²⁾H₄O₆I

Chemical Property of C₂₉H₂₇⁽²⁾H₄O₆I

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₂₉H₂₇⁽²⁾H₄O₆I

There total 6 articles about C₂₉H₂₇⁽²⁾H₄O₆I which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C31H27(2)H7O8 (945033-11-4) → C29H27(2)H4O6I (945033-20-5)

Guidance literature:

With trimethylsilyl iodide; In dichloromethane; at 0 ℃;

DOI:10.1021/jo070229y

Reference yield:

6-O-acetyl-2,3,4-tri-O-benzyl-D-manno-1,5-lactone (878270-46-3) → C29H27(2)H4O6I (945033-20-5)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium borodeuteride / methanol; H₂O / 0.05 h / 0 °C

2: sodium methoxide / methanol / 0.5 h / 0 - 10 °C

3: 81 percent / pyridine / 4 h / 20 °C

4: trimethylsilyl iodide / CH₂Cl₂ / 0 °C

With pyridine; sodium borodeuteride; trimethylsilyl iodide; sodium methylate; In methanol; dichloromethane; water;

DOI:10.1021/jo070229y

Reference yield:

1-deutero-6-O-acetyl-2,3,4-tri-O-benzyl-α-D-mannopyranose (945033-08-9) → C29H27(2)H4O6I (945033-20-5)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium methoxide / methanol / 0.5 h / 0 - 10 °C

2: 81 percent / pyridine / 4 h / 20 °C

3: trimethylsilyl iodide / CH₂Cl₂ / 0 °C

With pyridine; trimethylsilyl iodide; sodium methylate; In methanol; dichloromethane;

DOI:10.1021/jo070229y

upstream raw materials:

C₃₁H₂₇⁽²⁾H₇O₈

6-O-acetyl-2,3,4-tri-O-benzyl-D-manno-1,5-lactone

1-deutero-6-O-acetyl-2,3,4-tri-O-benzyl-α-D-mannopyranose

1-deutero-2,3,4-tri-O-benzyl-α-D-mannopyranose