1-benzyl-1'-N,N-dimethylaminomethylferrocene

Base Information

Chemical Name:1-benzyl-1'-N,N-dimethylaminomethylferrocene
CAS No.:767321-33-5
Molecular Formula:C₂₀H₂₃FeN
Molecular Weight:333.256
Hs Code.:

Synonyms:1-benzyl-1'-N,N-dimethylaminomethylferrocene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-benzyl-1'-N,N-dimethylaminomethylferrocene

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Technology Process of 1-benzyl-1'-N,N-dimethylaminomethylferrocene

There total 1 articles about 1-benzyl-1'-N,N-dimethylaminomethylferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 767321-31-3
1-benzoyl-1'-N,N-dimethylferrocenecarboxamide

: 767321-33-5
1-benzyl-1'-N,N-dimethylaminomethylferrocene

Guidance literature:: With AlCl₃; LiAlH₄; In diethyl ether; a soln. of AlCl3 in ether was added dropwise to a suspn. of LiAlH4 in ether, a soln. of complex in ether was added dropwise, the mixt. was refluxed for 2 h; H2O was added, 2 M NaOH, the water layer was extd. with ether, dired with MgSO4, concd., flahs column chromd. (silica gel, acetone-hexanes with 1% Et3N); an oil was solidified under high vac., crystd. from hexanes for 3 weeks at 0°C; elem. anal.;
DOI:10.1039/b313422a

Reference yield: 90.0%

: 767321-33-5
1-benzyl-1'-N,N-dimethylaminomethylferrocene

: 74-88-4
methyl iodide

: 767321-30-2
1-benzyl-1'-N,N-dimethylaminomethylferrocene methiodide

Guidance literature:: In dichloromethane; a soln. in CH2Cl2 was stirred at room temp. overnight; concd., washed with ether, maintained under high vac. for 16 h, crystd. from acetone; elem. anal.;
DOI:10.1039/b313422a