1,3-bis((trimethylsilyl)oxy)-2-(4-iodophenyl)-4,4,5,5-tetramethyl-1,3-imidazolidine

Base Information

• Chemical Name: 1,3-bis((trimethylsilyl)oxy)-2-(4-iodophenyl)-4,4,5,5-tetramethyl-1,3-imidazolidine
• CAS No.: 1454794-27-4
• Molecular Formula: C₁₉H₃₅IN₂O₂Si₂
• Molecular Weight: 506.575

Synonyms:1,3-bis((trimethylsilyl)oxy)-2-(4-iodophenyl)-4,4,5,5-tetramethyl-1,3-imidazolidine

Chemical Property of 1,3-bis((trimethylsilyl)oxy)-2-(4-iodophenyl)-4,4,5,5-tetramethyl-1,3-imidazolidine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3-bis((trimethylsilyl)oxy)-2-(4-iodophenyl)-4,4,5,5-tetramethyl-1,3-imidazolidine

There total 3 articles about 1,3-bis((trimethylsilyl)oxy)-2-(4-iodophenyl)-4,4,5,5-tetramethyl-1,3-imidazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3-bis(hydroxyamino)-2,3-dimethylbutane monosulfate (14538-51-3,78375-92-5) → 1,3-bis((trimethylsilyl)oxy)-2-(4-iodophenyl)-4,4,5,5-tetramethyl-1,3-imidazolidine (1454794-27-4)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / methanol / 6 h / Reflux

2: triethylamine / 20 h / 20 - 45 °C

With potassium carbonate; triethylamine; In methanol;

DOI:10.1021/jo4015062

Reference yield:

p-(iodophenyl)carboxaldehyde (15164-44-0) → 1,3-bis((trimethylsilyl)oxy)-2-(4-iodophenyl)-4,4,5,5-tetramethyl-1,3-imidazolidine (1454794-27-4)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / methanol / 6 h / Reflux

2: triethylamine / 20 h / 20 - 45 °C

With potassium carbonate; triethylamine; In methanol;

DOI:10.1021/jo4015062

Reference yield:

chloro-trimethyl-silane (75-77-4) + 2-(4-iodophenyl)-4,4,5,5-tetramethylimidazolidine-1,3-diol → 1,3-bis((trimethylsilyl)oxy)-2-(4-iodophenyl)-4,4,5,5-tetramethyl-1,3-imidazolidine (1454794-27-4)

Guidance literature:

With triethylamine; at 20 - 45 ℃; for 20h;

DOI:10.1021/jo4015062

upstream raw materials:

chloro-trimethyl-silane

p-(iodophenyl)carboxaldehyde

2,3-bis(hydroxyamino)-2,3-dimethylbutane monosulfate

Downstream raw materials:

1,4-bis(2-(2,5-dibutoxy-4-(2-(4-(4,4,5,5-tetramethyl-1,3-bis-((trimethylsilyl)oxy)imidazolidin-2-yl)phenyl)ethynyl)phenyl)-ethynyl)-2,5-dibutoxybenzene

1,4-bis(2-(2,5-dibutoxy-4-(2-(2,5-dibutoxy-4-(2-(4-(4,4,5,5-tetramethyl-1,3-bis((trimethylsilyl)oxy)imidazolidin-2-yl)phenyl)ethynyl)-phenyl)ethynyl)phenyl)ethynyl)-2,5-dibutoxybenzene

1,2-bis(2,5-dibutoxy-4-(2-(4-(4,4,5,5-tetramethyl-1,3-bis-((trimethylsilyl)oxy)imidazolidin-2-yl)phenyl)ethynyl)phenyl)ethyne

1,2-bis(2,5-dibutoxy-4-(2-(4-(1-oxyl-3-oxide-4,4,5,5-tetramethylimidazolin-2-yl)phenyl)ethynyl)phenyl)ethyne

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1454794-27-4 1,3-bis((trimethylsilyl)oxy)-2-(4-iodophenyl)-4,4,5,5-tetramethyl-1,3-imidazolidine

Send

Send

Metric Ton KG G Pound L ML

Send

Send