6-N-benzyloxycarbonyl-2',3'-O-benzylideneadenosine

Base Information

Chemical Name:6-N-benzyloxycarbonyl-2',3'-O-benzylideneadenosine
CAS No.:1356085-12-5
Molecular Formula:C₂₅H₂₃N₅O₆
Molecular Weight:489.488
Hs Code.:

Synonyms:6-N-benzyloxycarbonyl-2',3'-O-benzylideneadenosine

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Chemical Property of 6-N-benzyloxycarbonyl-2',3'-O-benzylideneadenosine

Chemical Property:

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Technology Process of 6-N-benzyloxycarbonyl-2',3'-O-benzylideneadenosine

There total 4 articles about 6-N-benzyloxycarbonyl-2',3'-O-benzylideneadenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1356085-09-0
6-N-benzyloxycarbonyl-2',3'-O-benzylidene-5'-O-(tert-butyldimethylsilyl)adenosine

: 1356085-12-5
6-N-benzyloxycarbonyl-2',3'-O-benzylideneadenosine

Guidance literature:: 6-N-benzyloxycarbonyl-2',3'-O-benzylidene-5'-O-(tert-butyldimethylsilyl)adenosine; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

With pyridine; In tetrahydrofuran;
DOI:10.1016/j.tet.2011.12.011

Reference yield:

: 3257-69-0
2',3'-O,O-benzylidene adenosine

: 1356085-12-5
6-N-benzyloxycarbonyl-2',3'-O-benzylideneadenosine

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine; 1H-imidazole / 24 h / 20 °C / Inert atmosphere

2.1: dichloromethane / 24 h / 20 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

3.2: Dowex x 50w

With pyridine; 1H-imidazole; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tet.2011.12.011

Reference yield:

: 100-52-7
benzaldehyde

: 1356085-12-5
6-N-benzyloxycarbonyl-2',3'-O-benzylideneadenosine

Guidance literature:: Multi-step reaction with 4 steps

1.1: zinc(II) chloride / 72 h / 20 °C / Inert atmosphere

2.1: pyridine; 1H-imidazole / 24 h / 20 °C / Inert atmosphere

3.1: dichloromethane / 24 h / 20 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

4.2: Dowex x 50w

With pyridine; 1H-imidazole; tetrabutyl ammonium fluoride; zinc(II) chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tet.2011.12.011