tert-butyl (1-(4-bromophenyl)-3-((2-(hydroxymethyl)benzyl)oxy)propan-2-yl)carbamate

Base Information

Chemical Name:tert-butyl (1-(4-bromophenyl)-3-((2-(hydroxymethyl)benzyl)oxy)propan-2-yl)carbamate
CAS No.:1333114-54-7
Molecular Formula:C₂₂H₂₈BrNO₄
Molecular Weight:450.373
Hs Code.:

Synonyms:tert-butyl (1-(4-bromophenyl)-3-((2-(hydroxymethyl)benzyl)oxy)propan-2-yl)carbamate

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Chemical Property of tert-butyl (1-(4-bromophenyl)-3-((2-(hydroxymethyl)benzyl)oxy)propan-2-yl)carbamate

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Technology Process of tert-butyl (1-(4-bromophenyl)-3-((2-(hydroxymethyl)benzyl)oxy)propan-2-yl)carbamate

There total 7 articles about tert-butyl (1-(4-bromophenyl)-3-((2-(hydroxymethyl)benzyl)oxy)propan-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89-71-4
2-Methyl-benzoic acid methyl ester

: 1333114-54-7
tert-butyl (1-(4-bromophenyl)-3-((2-(hydroxymethyl)benzyl)oxy)propan-2-yl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide; dibenzoyl peroxide / chloroform / Reflux

2.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 °C

2.2: 20 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0.5 h / 0 °C

With N-Bromosuccinimide; lithium aluminium tetrahydride; sodium hydride; dibenzoyl peroxide; In tetrahydrofuran; diethyl ether; chloroform; mineral oil;

Reference yield:

: 118-90-1
ortho-methylbenzoic acid

: 1333114-54-7
tert-butyl (1-(4-bromophenyl)-3-((2-(hydroxymethyl)benzyl)oxy)propan-2-yl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride / 70 °C

2.1: N-Bromosuccinimide / 2,2'-azobis(isobutyronitrile) / tetrachloromethane / Reflux

3.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 °C

3.2: 20 °C

4.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0.5 h / 0 °C

With hydrogenchloride; N-Bromosuccinimide; lithium aluminium tetrahydride; sodium hydride; 2,2'-azobis(isobutyronitrile); In tetrahydrofuran; tetrachloromethane; diethyl ether; mineral oil;

Reference yield:

: 132067-41-5
methyl (±)-3-(4-bromophenyl)-2-((tert-butoxycarbonyl)amino)propanoate

: 1333114-54-7
tert-butyl (1-(4-bromophenyl)-3-((2-(hydroxymethyl)benzyl)oxy)propan-2-yl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium tetrahydroborate; lithium chloride hydrate / tetrahydrofuran; ethanol / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 °C

2.2: 20 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0.5 h / 0 °C

With sodium tetrahydroborate; lithium aluminium tetrahydride; lithium chloride hydrate; sodium hydride; In tetrahydrofuran; diethyl ether; ethanol; mineral oil;