{(P(C₂H₅)3)2HPt(H)2Pt(P(C₂H₅)3)2}⁽¹⁺⁾*B(C₆H₅)4^(1-)={(P(C₂H₅)3)2HPt(H)2Pt(P(C₂H₅)3)2}{B(C₆H₅)4}

Base Information

• Chemical Name: {(P(C₂H₅)3)2HPt(H)2Pt(P(C₂H₅)3)2}⁽¹⁺⁾*B(C₆H₅)4^(1-)={(P(C₂H₅)3)2HPt(H)2Pt(P(C₂H₅)3)2}{B(C₆H₅)4}
• CAS No.: 81800-05-7
• Molecular Formula: C₂₄H₂₀B*C₂₄H₆₃P₄Pt₂
• Molecular Weight: 1185.05

Synonyms:{(P(C₂H₅)3)2HPt(H)2Pt(P(C₂H₅)3)2}⁽¹⁺⁾*B(C₆H₅)4^(1-)={(P(C₂H₅)3)2HPt(H)2Pt(P(C₂H₅)3)2}{B(C₆H₅)4}

Chemical Property of {(P(C₂H₅)3)2HPt(H)2Pt(P(C₂H₅)3)2}⁽¹⁺⁾*B(C₆H₅)4^(1-)={(P(C₂H₅)3)2HPt(H)2Pt(P(C₂H₅)3)2}{B(C₆H₅)4}

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Technology Process of {(P(C₂H₅)3)2HPt(H)2Pt(P(C₂H₅)3)2}⁽¹⁺⁾*B(C₆H₅)4^(1-)={(P(C₂H₅)3)2HPt(H)2Pt(P(C₂H₅)3)2}{B(C₆H₅)4}

There total 4 articles about {(P(C₂H₅)3)2HPt(H)2Pt(P(C₂H₅)3)2}⁽¹⁺⁾*B(C₆H₅)4^(1-)={(P(C₂H₅)3)2HPt(H)2Pt(P(C₂H₅)3)2}{B(C₆H₅)4} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

(Pt2(μ-H)2H(PEt3)4)(HCO2) (81800-04-6) + sodium tetraphenyl borate (143-66-8) → {(P(C2H5)3)2HPt(H)2Pt(P(C2H5)3)2}(1+)*B(C6H5)4(1-)={(P(C2H5)3)2HPt(H)2Pt(P(C2H5)3)2}{B(C6H5)4} (81800-05-7) + sodium formate (141-53-7)

Guidance literature:

In acetonitrile; NaBPh4 added to soln. (Pt2(μ-H)2HPt(PEt3)4)(HCO2) in acetonitrile; ppt. filtered, solvent removed under vac., residue dissolved in acetone, methanol added and soln. cooled to -10°C for 48 h; elem. anal.;

Reference yield:

{(P(C2H5)3)2HPt(H)PtH(P(C2H5)3)2}(1+)*B(C6H5)4(1-)={(P(C2H5)3)2HPtHPtH(P(C2H5)3)2}{B(C6H5)4} (84624-72-6) → {(P(C2H5)3)2HPt(H)2Pt(P(C2H5)3)2}(1+)*B(C6H5)4(1-)={(P(C2H5)3)2HPt(H)2Pt(P(C2H5)3)2}{B(C6H5)4} (81800-05-7)

Guidance literature:

With tetra-(n-butyl)ammonium iodide; In [⁽²⁾H₆]acetone; soln. complex in acetone-d6 and 1 equiv. (n-Bu)4NI stirred at 25°C;

Reference yield:

{Pt2H3(P(C2H5)3)4}(1+)*{HCO2}(1-)={Pt2H3(P(C2H5)3)4}{HCO2} (81800-04-6) + sodium tetraphenyl borate (143-66-8) → {Pt2H3(P(C2H5)3)4}(1+)*{B(C6H5)4}(1-)={Pt2H3(P(C2H5)3)4}{B(C6H5)4} (81800-05-7)

Guidance literature:

In not given; metathesis;

DOI:10.1021/ja00376a058

upstream raw materials:

(Pt2(μ-H)2H(PEt3)4)(HCO2)

sodium tetraphenyl borate

{(P(C₂H₅)3)2HPt(H)PtH(P(C₂H₅)3)2}⁽¹⁺⁾*B(C₆H₅)4^(1-)={(P(C₂H₅)3)2HPtHPtH(P(C₂H₅)3)2}{B(C₆H₅)4}

{Pt₂H₃(P(C₂H₅)3)4}⁽¹⁺⁾*{HCO₂}^(1-)={Pt₂H₃(P(C₂H₅)3)4}{HCO₂}

Downstream raw materials:

tris(triethylphosphine)platinum⁽⁰⁾

hydridotris(triethylphosphine)platinum(II) tetraphenylborate

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