C₂₅H₂₆N₄O₂

Base Information

Chemical Name:C₂₅H₂₆N₄O₂
CAS No.:1093133-04-0
Molecular Formula:C₂₅H₂₆N₄O₂
Molecular Weight:414.507
Hs Code.:

C<sub>25</sub>H<sub>26</sub>N<sub>4</sub>O<sub>2</sub>

Synonyms:C₂₅H₂₆N₄O₂

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Chemical Property of C₂₅H₂₆N₄O₂

Chemical Property:

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Technology Process of C₂₅H₂₆N₄O₂

There total 6 articles about C₂₅H₂₆N₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1403950-74-2
C₃₃H₃₀N₄O₅

: 1093133-04-0
C₂₅H₂₆N₄O₂

Guidance literature:: C₃₃H₃₀N₄O₅; With hydrazine hydrate; In methanol; acetonitrile; at 20 ℃; for 2h; Inert atmosphere;

With phosphorus pentoxide; In ethanol; at 80 ℃; Acidic conditions;
DOI:10.1021/ml300209g

Reference yield:

: 1093134-17-8
C₁₉H₃₁NO₂Si

: 1093133-04-0
C₂₅H₂₆N₄O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: tert.-butyl lithium / tetrahydrofuran / 0.75 h / -78 °C / Inert atmosphere

2.1: Burgess Reagent / tetrahydrofuran / 0.75 h / 20 - 80 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

4.1: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / tetrahydrofuran / 20 - 80 °C / Inert atmosphere

5.1: hydrazine hydrate / methanol; acetonitrile / 2 h / 20 °C / Inert atmosphere

5.2: 80 °C / Acidic conditions

With Burgess Reagent; hydrazine hydrate; tributylphosphine; tetrabutyl ammonium fluoride; tert.-butyl lithium; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; methanol; acetonitrile; 4.1: |Mitsunobu Displacement;
DOI:10.1021/ml300209g

Reference yield:

: 120417-13-2
(S)-2-(tert-butyldimethylsilyloxy)-1-phenylethylamine

: 1093133-04-0
C₂₅H₂₆N₄O₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine / dichloromethane / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide / 20 - 60 °C / Inert atmosphere

3.1: tert.-butyl lithium / tetrahydrofuran / 0.75 h / -78 °C / Inert atmosphere

4.1: Burgess Reagent / tetrahydrofuran / 0.75 h / 20 - 80 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

6.1: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / tetrahydrofuran / 20 - 80 °C / Inert atmosphere

7.1: hydrazine hydrate / methanol; acetonitrile / 2 h / 20 °C / Inert atmosphere

7.2: 80 °C / Acidic conditions

With Burgess Reagent; hydrazine hydrate; tributylphosphine; tetrabutyl ammonium fluoride; tert.-butyl lithium; sodium hydride; triethylamine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 6.1: |Mitsunobu Displacement;
DOI:10.1021/ml300209g