2,5-dimethyl-4,6-dinitroanisole

Base Information

• Chemical Name: 2,5-dimethyl-4,6-dinitroanisole
• CAS No.: 133426-94-5
• Molecular Formula: C₉H₁₀N₂O₅
• Molecular Weight: 226.189
• Mol file: 133426-94-5.mol

Synonyms:2,5-dimethyl-4,6-dinitroanisole

Chemical Property of 2,5-dimethyl-4,6-dinitroanisole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,5-dimethyl-4,6-dinitroanisole

There total 4 articles about 2,5-dimethyl-4,6-dinitroanisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

2,5-Dimethyl-anisol (1706-11-2) → 2,5-dimethyl-4,6-dinitroanisole (133426-94-5)

Guidance literature:

With trifluoroacetic acid; sodium nitrite; for 24h; Ambient temperature;

DOI:10.1021/jo981143v

Reference yield: 65.0%

1-methoxy-2,5-dimethyl-4-nitrobenzene (3139-06-8) → 2,5-dimethyl-4,6-dinitroanisole (133426-94-5)

Guidance literature:

With nitric acid; for 2h; Ambient temperature;

DOI:10.1016/S0040-4020(01)87932-1

Reference yield:

sodium methylate (124-41-4) → 2,5-dimethyl-4,6-dinitroanisole (133426-94-5)

Guidance literature:

With methanol;

upstream raw materials:

2,3,5-trinitro-p-xylene

sodium methylate

1-methoxy-2,5-dimethyl-4-nitrobenzene

2,5-Dimethyl-anisol

Downstream raw materials:

methyl 3-(3-methoxy-4-methyl-2,6-dinitrophenyl)-2-oxopropanoate

ethyl N-(2,5-dimethyl-4-methoxy-3-nitrophenyl)-formimidate

2,5-dimethyl-4-methoxy-3-nitroaniline

Refernces

• 1、 Dong,Jimenez. "Synthesis of a fully functionalized 7-methoxyaziridinomitosene". . p. 2520 - 2523. Retrieved 2007/10/03.