S-4-(1,1,1-trifluoro-2-hydroxypropan-2-yl)phenyl dimethylcarbamothioate

Base Information

Chemical Name:S-4-(1,1,1-trifluoro-2-hydroxypropan-2-yl)phenyl dimethylcarbamothioate
CAS No.:869854-54-6
Molecular Formula:C₁₂H₁₄F₃NO₂S
Molecular Weight:293.31
Hs Code.:

Synonyms:S-4-(1,1,1-trifluoro-2-hydroxypropan-2-yl)phenyl dimethylcarbamothioate

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Chemical Property of S-4-(1,1,1-trifluoro-2-hydroxypropan-2-yl)phenyl dimethylcarbamothioate

Chemical Property:

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Technology Process of S-4-(1,1,1-trifluoro-2-hydroxypropan-2-yl)phenyl dimethylcarbamothioate

There total 3 articles about S-4-(1,1,1-trifluoro-2-hydroxypropan-2-yl)phenyl dimethylcarbamothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10345-50-3
O-(4-acetylphenyl) N,N-dimethylcarbamothioate

: 81290-20-2
(trifluoromethyl)trimethylsilane

: 869854-54-6
S-4-(1,1,1-trifluoro-2-hydroxypropan-2-yl)phenyl dimethylcarbamothioate

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at -5 - 15 ℃; for 0.583333h;

Reference yield:

: 10345-50-3
O-(4-acetylphenyl) N,N-dimethylcarbamothioate

: 869854-54-6
S-4-(1,1,1-trifluoro-2-hydroxypropan-2-yl)phenyl dimethylcarbamothioate

Guidance literature:: Multi-step reaction with 2 steps

1: neat (no solvent) / 192 - 218 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.58 h / -5 - 15 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1021/ml500331y

Reference yield:

: 99-93-4
4-Hydroxyacetophenone

: 869854-54-6
S-4-(1,1,1-trifluoro-2-hydroxypropan-2-yl)phenyl dimethylcarbamothioate

Guidance literature:: Multi-step reaction with 3 steps

1: 1,4-diaza-bicyclo[2.2.2]octane / N,N-dimethyl-formamide / 1 h / Inert atmosphere

2: neat (no solvent) / 192 - 218 °C / Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.58 h / -5 - 15 °C / Inert atmosphere

With 1,4-diaza-bicyclo[2.2.2]octane; tetrabutyl ammonium fluoride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ml500331y