4,5-di-O-benzoyl-1-O-tert-butyldiphenylsilyl-2,3-O-cyclohexylidene-6-O-methoxymethyl-myo-inositol

Base Information

Chemical Name:4,5-di-O-benzoyl-1-O-tert-butyldiphenylsilyl-2,3-O-cyclohexylidene-6-O-methoxymethyl-myo-inositol
CAS No.:1412439-56-5
Molecular Formula:C₄₄H₅₀O₉Si
Molecular Weight:750.961
Hs Code.:

Synonyms:4,5-di-O-benzoyl-1-O-tert-butyldiphenylsilyl-2,3-O-cyclohexylidene-6-O-methoxymethyl-myo-inositol

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Chemical Property of 4,5-di-O-benzoyl-1-O-tert-butyldiphenylsilyl-2,3-O-cyclohexylidene-6-O-methoxymethyl-myo-inositol

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Technology Process of 4,5-di-O-benzoyl-1-O-tert-butyldiphenylsilyl-2,3-O-cyclohexylidene-6-O-methoxymethyl-myo-inositol

There total 6 articles about 4,5-di-O-benzoyl-1-O-tert-butyldiphenylsilyl-2,3-O-cyclohexylidene-6-O-methoxymethyl-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1412439-55-4
1-O-tert-butyldiphenylsilyl-2,3-O-cyclohexylidene-6-O-methoxymethyl-myo-inositol

: 98-88-4
benzoyl chloride

: 1412439-56-5
4,5-di-O-benzoyl-1-O-tert-butyldiphenylsilyl-2,3-O-cyclohexylidene-6-O-methoxymethyl-myo-inositol

Guidance literature:: In pyridine; dichloromethane; at 0 - 20 ℃; for 24h; Inert atmosphere;
DOI:10.1002/ejoc.201200726

Reference yield:

: 1412439-52-1
1-[1-(S)-camphanyl]-2,3:4,5-di-O-cyclohexylidene-6-O-methoxymethyl-myo-inositol

: 1412439-56-5
4,5-di-O-benzoyl-1-O-tert-butyldiphenylsilyl-2,3-O-cyclohexylidene-6-O-methoxymethyl-myo-inositol

Guidance literature:: Multi-step reaction with 4 steps

1: lithium hydroxide / water; tetrahydrofuran / 1 h / 20 °C

2: 1H-imidazole / pyridine / 120 h / 65 °C / Inert atmosphere

3: acetyl chloride / dichloromethane; methanol / 1.5 h / 0 °C

4: pyridine; dichloromethane / 24 h / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; acetyl chloride; lithium hydroxide; In tetrahydrofuran; pyridine; methanol; dichloromethane; water;
DOI:10.1002/ejoc.201200726

Reference yield:

: C₂₈H₄₀O₉

: 1412439-56-5
4,5-di-O-benzoyl-1-O-tert-butyldiphenylsilyl-2,3-O-cyclohexylidene-6-O-methoxymethyl-myo-inositol

Guidance literature:: Multi-step reaction with 5 steps

1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 72 h / 20 °C / Inert atmosphere

2: lithium hydroxide / water; tetrahydrofuran / 1 h / 20 °C

3: 1H-imidazole / pyridine / 120 h / 65 °C / Inert atmosphere

4: acetyl chloride / dichloromethane; methanol / 1.5 h / 0 °C

5: pyridine; dichloromethane / 24 h / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; N-ethyl-N,N-diisopropylamine; acetyl chloride; lithium hydroxide; In tetrahydrofuran; pyridine; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201200726