2,4-Bis-(4-methoxy-benzoyl)-1,5-bis-(4-methoxy-phenyl)-pentane-1,5-dione

Base Information

Chemical Name:2,4-Bis-(4-methoxy-benzoyl)-1,5-bis-(4-methoxy-phenyl)-pentane-1,5-dione
CAS No.:170647-10-6
Molecular Formula:C₃₅H₃₂O₈
Molecular Weight:580.634
Hs Code.:

Synonyms:2,4-Bis-(4-methoxy-benzoyl)-1,5-bis-(4-methoxy-phenyl)-pentane-1,5-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,4-Bis-(4-methoxy-benzoyl)-1,5-bis-(4-methoxy-phenyl)-pentane-1,5-dione

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Technology Process of 2,4-Bis-(4-methoxy-benzoyl)-1,5-bis-(4-methoxy-phenyl)-pentane-1,5-dione

There total 3 articles about 2,4-Bis-(4-methoxy-benzoyl)-1,5-bis-(4-methoxy-phenyl)-pentane-1,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 18362-51-1
1,3-bis(4'-methoxyphenyl)propane-1,3-dione

: 170647-10-6
2,4-Bis-(4-methoxy-benzoyl)-1,5-bis-(4-methoxy-phenyl)-pentane-1,5-dione

Guidance literature:: hydroxocobalt(III) Schiff base; In dichloromethane; at 25 ℃; for 48h;
DOI:10.1016/00404-0399(50)1074R-

Reference yield: 89.0%

: 109-86-4,95507-80-5
2-methoxy-ethanol

: 18362-51-1
1,3-bis(4'-methoxyphenyl)propane-1,3-dione

: 170647-10-6
2,4-Bis-(4-methoxy-benzoyl)-1,5-bis-(4-methoxy-phenyl)-pentane-1,5-dione

Guidance literature:: With oxygen; sodium hydrogencarbonate; at 65 ℃; Sealed tube;
DOI:10.1039/d1ob02290c

Reference yield:

: 65418-71-5
1,3-bis-(4-methoxyphenyl)-2-ethynyl-1-one

: 170647-10-6
2,4-Bis-(4-methoxy-benzoyl)-1,5-bis-(4-methoxy-phenyl)-pentane-1,5-dione

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid; water / toluene / 70 °C / Sealed tube

2: sodium hydrogencarbonate; oxygen / 65 °C / Sealed tube

With water; oxygen; sodium hydrogencarbonate; toluene-4-sulfonic acid; In toluene;
DOI:10.1039/d1ob02290c