dithiophenylglyoxime

Base Information

Chemical Name:dithiophenylglyoxime
CAS No.:57501-54-9
Molecular Formula:C₁₄H₁₂N₂O₂S₂
Molecular Weight:304.393
Hs Code.:

Synonyms:dithiophenylglyoxime

Suppliers and Price of dithiophenylglyoxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dithiophenylglyoxime

Chemical Property:

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Technology Process of dithiophenylglyoxime

There total 1 articles about dithiophenylglyoxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-98-5
thiophenol

: 2038-44-0
dichloroglyoxime

: 57501-54-9
dithiophenylglyoxime

Guidance literature:: With potassium carbonate; potassium hydroxide;
DOI:10.1016/j.jorganchem.2010.10.066

Reference yield: 73.0%

: 110-86-1
pyridine

: cobalt(II) chloride hexahydrate

: 57501-54-9
dithiophenylglyoxime

: 1159404-38-2
CoCl((bis(thiophenyl)glyoxime-H)2(pyridine)

Guidance literature:: With air; In ethanol; Co compd. (0.420 mmol) added to soln. of dithiophenylglyoxime (0.840 mmol) in EtOH under stirring, stirring for 10-15 min, heating for 8-10 min with a hot air gun, C5H5N (0.783 mmol) added dropwise, air passed through soln. for 0.5 h; solid filtered off, washed with water and dried over P2O5 overnight, column chromy. (silica gel, CH2Cl2); elem. anal.;
DOI:10.1021/om900065k

Reference yield:

: 57501-54-9
dithiophenylglyoxime

: Co(O₂)(benzyl)(pyridine)(dithiophenylglyoxime(-1H))(dimethylglyoxime(-1H))

Guidance literature:: Multi-step reaction with 3 steps

1: air / ethanol

2: NaBH₄ / not given

With air; NaBH₄; In ethanol;
DOI:10.1016/j.jorganchem.2011.02.033