(7R,8R)-3-Methyl-9-oxo-8-(2-phenoxy-acetylamino)-6-thia-1-aza-bicyclo[5.2.0]non-2-ene-2,5,5-tricarboxylic acid dimethyl ester

Base Information

Chemical Name:(7R,8R)-3-Methyl-9-oxo-8-(2-phenoxy-acetylamino)-6-thia-1-aza-bicyclo[5.2.0]non-2-ene-2,5,5-tricarboxylic acid dimethyl ester
CAS No.:130994-97-7
Molecular Formula:C₂₁H₂₂N₂O₉S
Molecular Weight:478.48
Hs Code.:

Synonyms:(7R,8R)-3-Methyl-9-oxo-8-(2-phenoxy-acetylamino)-6-thia-1-aza-bicyclo[5.2.0]non-2-ene-2,5,5-tricarboxylic acid dimethyl ester

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Chemical Property of (7R,8R)-3-Methyl-9-oxo-8-(2-phenoxy-acetylamino)-6-thia-1-aza-bicyclo[5.2.0]non-2-ene-2,5,5-tricarboxylic acid dimethyl ester

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Technology Process of (7R,8R)-3-Methyl-9-oxo-8-(2-phenoxy-acetylamino)-6-thia-1-aza-bicyclo[5.2.0]non-2-ene-2,5,5-tricarboxylic acid dimethyl ester

There total 4 articles about (7R,8R)-3-Methyl-9-oxo-8-(2-phenoxy-acetylamino)-6-thia-1-aza-bicyclo[5.2.0]non-2-ene-2,5,5-tricarboxylic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: (7R,8R)-3-Methyl-9-oxo-8-(2-phenoxy-acetylamino)-6-thia-1-aza-bicyclo[5.2.0]non-2-ene-2,5,5-tricarboxylic acid dimethyl ester 4-nitro-benzyl ester

: 130994-97-7
(7R,8R)-3-Methyl-9-oxo-8-(2-phenoxy-acetylamino)-6-thia-1-aza-bicyclo[5.2.0]non-2-ene-2,5,5-tricarboxylic acid dimethyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol;

Reference yield:

: 60761-30-0
(6R)-3-methylene-8-oxo-7t-(2-phenoxy-acetylamino)-(6rH)-5-thia-1-aza-bicyclo[4.2.0]octane-2c-carboxylic acid 4-nitro-benzyl ester

: 130994-97-7
(7R,8R)-3-Methyl-9-oxo-8-(2-phenoxy-acetylamino)-6-thia-1-aza-bicyclo[5.2.0]non-2-ene-2,5,5-tricarboxylic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / CuSO₄ / various solvent(s) / Heating

2: 92 percent / Et₃N / CH₂Cl₂

3: 84 percent / H₂ / Pd/C / tetrahydrofuran; methanol

With hydrogen; copper(II) sulfate; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 6773-29-1
dimethyl diazomalonate

: 130994-97-7
(7R,8R)-3-Methyl-9-oxo-8-(2-phenoxy-acetylamino)-6-thia-1-aza-bicyclo[5.2.0]non-2-ene-2,5,5-tricarboxylic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / CuSO₄ / various solvent(s) / Heating

2: 92 percent / Et₃N / CH₂Cl₂

3: 84 percent / H₂ / Pd/C / tetrahydrofuran; methanol

With hydrogen; copper(II) sulfate; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;