N-(2,6-difluorophenyl)trimethylacetamide

Base Information

• Chemical Name: N-(2,6-difluorophenyl)trimethylacetamide
• CAS No.: 1240020-41-0
• Molecular Formula: C₁₁H₁₃F₂NO
• Molecular Weight: 213.227

Synonyms:N-(2,6-difluorophenyl)trimethylacetamide

Chemical Property of N-(2,6-difluorophenyl)trimethylacetamide

Chemical Property:

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Technology Process of N-(2,6-difluorophenyl)trimethylacetamide

There total 1 articles about N-(2,6-difluorophenyl)trimethylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2,6-difluoroaniline (5509-65-9) + pivaloyl chloride (3282-30-2) → N-(2,6-difluorophenyl)trimethylacetamide (1240020-41-0)

Guidance literature:

With triethylamine; In toluene; at 0 - 50 ℃;

Reference yield:

iodobenzene (591-50-4) + N-(2,6-difluorophenyl)trimethylacetamide (1240020-41-0) → C17H17F2NO (1240020-43-2) + C23H21F2NO (1240020-44-3) + C29H25F2NO (1240020-45-4)

Guidance literature:

With silver(I) acetate; palladium diacetate; caesium carbonate; at 130 ℃; for 3h;

DOI:10.1016/j.tet.2010.03.111

upstream raw materials:

2,6-difluoroaniline

pivaloyl chloride

Downstream raw materials:

C₁₇H₁₇F₂NO

C₂₃H₂₁F₂NO

C₂₉H₂₅F₂NO

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