(2S,3R)-3-(tert-Butyl-diphenyl-silanyloxy)-2-(2-methoxy-ethoxymethoxymethyl)-butan-1-ol

Base Information

Chemical Name:(2S,3R)-3-(tert-Butyl-diphenyl-silanyloxy)-2-(2-methoxy-ethoxymethoxymethyl)-butan-1-ol
CAS No.:135589-02-5
Molecular Formula:C₂₅H₃₈O₅Si
Molecular Weight:446.659
Hs Code.:

Synonyms:(2S,3R)-3-(tert-Butyl-diphenyl-silanyloxy)-2-(2-methoxy-ethoxymethoxymethyl)-butan-1-ol

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Chemical Property of (2S,3R)-3-(tert-Butyl-diphenyl-silanyloxy)-2-(2-methoxy-ethoxymethoxymethyl)-butan-1-ol

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Technology Process of (2S,3R)-3-(tert-Butyl-diphenyl-silanyloxy)-2-(2-methoxy-ethoxymethoxymethyl)-butan-1-ol

There total 4 articles about (2S,3R)-3-(tert-Butyl-diphenyl-silanyloxy)-2-(2-methoxy-ethoxymethoxymethyl)-butan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: C₃₁H₅₂O₅Si₂

: 135589-02-5
(2S,3R)-3-(tert-Butyl-diphenyl-silanyloxy)-2-(2-methoxy-ethoxymethoxymethyl)-butan-1-ol

Guidance literature:: With pyridinium p-toluenesulfonate; In ethanol; at 65 ℃; for 4h;
DOI:10.1016/S0040-4039(00)97081-3

Reference yield:

: C₃₅H₅₂O₄Si₂

: 135589-02-5
(2S,3R)-3-(tert-Butyl-diphenyl-silanyloxy)-2-(2-methoxy-ethoxymethoxymethyl)-butan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / H₂, CaCO₃ / Pd-C / ethanol

2: 64 percent / Et₃N / acetonitrile / 28 h / Heating

3: 61 percent / pyridinium tosylate / ethanol / 4 h / 65 °C

With hydrogen; pyridinium p-toluenesulfonate; triethylamine; calcium carbonate; palladium on activated charcoal; In ethanol; acetonitrile;
DOI:10.1016/S0040-4039(00)97081-3

Reference yield:

: 135245-91-9
(2R,3R)-3-Benzyloxymethoxymethyl-4-(tert-butyl-dimethyl-silanyloxy)-butan-2-ol

: 135589-02-5
(2S,3R)-3-(tert-Butyl-diphenyl-silanyloxy)-2-(2-methoxy-ethoxymethoxymethyl)-butan-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / imidazole / dimethylformamide / 10 h / 85 °C

2: 71 percent / H₂, CaCO₃ / Pd-C / ethanol

3: 64 percent / Et₃N / acetonitrile / 28 h / Heating

4: 61 percent / pyridinium tosylate / ethanol / 4 h / 65 °C

With 1H-imidazole; hydrogen; pyridinium p-toluenesulfonate; triethylamine; calcium carbonate; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4039(00)97081-3