2-[(Z)-2-(3,4-Dichloro-phenyl)-1-methoxycarbonyl-propenyl]-benzoic acid

Base Information

• Chemical Name: 2-[(Z)-2-(3,4-Dichloro-phenyl)-1-methoxycarbonyl-propenyl]-benzoic acid
• CAS No.: 79401-57-3
• Molecular Formula: C₁₈H₁₄Cl₂O₄
• Molecular Weight: 365.213

Synonyms:2-[(Z)-2-(3,4-Dichloro-phenyl)-1-methoxycarbonyl-propenyl]-benzoic acid

Chemical Property of 2-[(Z)-2-(3,4-Dichloro-phenyl)-1-methoxycarbonyl-propenyl]-benzoic acid

Chemical Property:

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Technology Process of 2-[(Z)-2-(3,4-Dichloro-phenyl)-1-methoxycarbonyl-propenyl]-benzoic acid

There total 2 articles about 2-[(Z)-2-(3,4-Dichloro-phenyl)-1-methoxycarbonyl-propenyl]-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dimethyl homophthalate (716-43-8) + 3',4'-dichloroacetophenone (2642-63-9) → 2-[(E)-2-(3,4-Dichloro-phenyl)-1-methoxycarbonyl-propenyl]-benzoic acid (79401-57-3) + 2-[(Z)-2-(3,4-Dichloro-phenyl)-1-methoxycarbonyl-propenyl]-benzoic acid (79401-57-3)

Guidance literature:

With sodium hydride; In benzene; at 50 - 70 ℃;

Reference yield:

dimethyl homophthalate (716-43-8) + 3',4'-dichloroacetophenone (2642-63-9) → 2-[(E)-2-(3,4-Dichloro-phenyl)-1-methoxycarbonyl-propenyl]-benzoic acid (79401-57-3) + 2-[(Z)-2-(3,4-Dichloro-phenyl)-1-methoxycarbonyl-propenyl]-benzoic acid (79401-57-3)

Guidance literature:

With sodium hydride; In benzene; at 50 - 70 ℃;

Reference yield: 85.0%

2-[(Z)-2-(3,4-Dichloro-phenyl)-1-methoxycarbonyl-propenyl]-benzoic acid (79401-57-3) → 2-(5,6-Dichloro-3-methyl-1-oxo-1H-inden-2-yl)-benzoic acid methyl ester (79401-68-6)

Guidance literature:

With acetic anhydride; zinc(II) chloride; In acetic acid; for 5h; Heating;

upstream raw materials:

dimethyl homophthalate

3',4'-dichloroacetophenone

Downstream raw materials:

2-[(E)-1-Carboxy-2-(3,4-dichloro-phenyl)-propenyl]-benzoic acid

2-(5,6-Dichloro-3-methyl-1-oxo-1H-inden-2-yl)-benzoic acid methyl ester

(3S,4R)-3-(3,4-Dichloro-phenyl)-3-methyl-1-oxo-isochroman-4-carboxylic acid methyl ester

4-[1-(3,4-Dichloro-phenyl)-eth-(Z)-ylidene]-isochroman-1,3-dione

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