4-methoxy-2-formyl trans-cinnamaldehyde

Base Information

• Chemical Name: 4-methoxy-2-formyl trans-cinnamaldehyde
• CAS No.: 1310720-11-6
• Molecular Formula: C₁₁H₁₀O₃
• Molecular Weight: 190.199
• Mol file: 1310720-11-6.mol

Synonyms:4-methoxy-2-formyl trans-cinnamaldehyde

Chemical Property of 4-methoxy-2-formyl trans-cinnamaldehyde

Chemical Property:

Purity/Quality:

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Technology Process of 4-methoxy-2-formyl trans-cinnamaldehyde

There total 2 articles about 4-methoxy-2-formyl trans-cinnamaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

C15H20O4 → 4-methoxy-2-formyl trans-cinnamaldehyde (1310720-11-6)

Guidance literature:

With hydrogenchloride; In water; acetone; at 20 ℃; for 0.5h;

DOI:10.1039/c6ob01918h

Reference yield:

2-bromo-5-methoxy-benzaldehyde (7507-86-0) → 4-methoxy-2-formyl trans-cinnamaldehyde (1310720-11-6)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrabutylammonium acetate; potassium carbonate; potassium chloride; palladium diacetate / N,N-dimethyl-formamide / 2 h / 90 °C

2: hydrogenchloride / water; acetone / 0.5 h / 20 °C

With hydrogenchloride; potassium chloride; tetrabutylammonium acetate; palladium diacetate; potassium carbonate; In water; N,N-dimethyl-formamide; acetone;

DOI:10.1039/c6ob01918h

upstream raw materials:

2-bromo-5-methoxy-benzaldehyde