2-[[(4-{2-[(1-benzofuran-2-ylcarbonyl)amino]ethoxy}phenyl)sulfonyl](benzyl)amino]-3,5-dimethylbenzoic acid

Base Information

Chemical Name:2-[[(4-{2-[(1-benzofuran-2-ylcarbonyl)amino]ethoxy}phenyl)sulfonyl](benzyl)amino]-3,5-dimethylbenzoic acid
CAS No.:306956-35-4
Molecular Formula:C₃₃H₃₀N₂O₇S
Molecular Weight:598.676
Hs Code.:

Synonyms:2-[[(4-{2-[(1-benzofuran-2-ylcarbonyl)amino]ethoxy}phenyl)sulfonyl](benzyl)amino]-3,5-dimethylbenzoic acid

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Chemical Property of 2-[[(4-{2-[(1-benzofuran-2-ylcarbonyl)amino]ethoxy}phenyl)sulfonyl](benzyl)amino]-3,5-dimethylbenzoic acid

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Technology Process of 2-[[(4-{2-[(1-benzofuran-2-ylcarbonyl)amino]ethoxy}phenyl)sulfonyl](benzyl)amino]-3,5-dimethylbenzoic acid

There total 2 articles about 2-[[(4-{2-[(1-benzofuran-2-ylcarbonyl)amino]ethoxy}phenyl)sulfonyl](benzyl)amino]-3,5-dimethylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 306956-34-3
benzofuran-2-carboxylic acid (2-hydroxyethyl)amide

: 206547-50-4
2-[Benzyl-(4-fluoro-benzenesulfonyl)-amino]-3,5-dimethyl-benzoic acid

: 306956-35-4
2-[[(4-{2-[(1-benzofuran-2-ylcarbonyl)amino]ethoxy}phenyl)sulfonyl](benzyl)amino]-3,5-dimethylbenzoic acid

Guidance literature:: benzofuran-2-carboxylic acid (2-hydroxyethyl)amide; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

2-[Benzyl-(4-fluoro-benzenesulfonyl)-amino]-3,5-dimethyl-benzoic acid; In N,N-dimethyl-formamide; at 0 - 20 ℃; Further stages.;
DOI:10.1021/ja001547g

Reference yield:

: 496-41-3
Benzofuran-2-carboxylic acid

: 306956-35-4
2-[[(4-{2-[(1-benzofuran-2-ylcarbonyl)amino]ethoxy}phenyl)sulfonyl](benzyl)amino]-3,5-dimethylbenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: 43 percent / HOBt; EDC; NMM / dimethylformamide / 4.17 h / 0 - 20 °C

2.1: NaH / dimethylformamide / 0.5 h / 0 °C

2.2: 58 percent / dimethylformamide / 0 - 20 °C

With 4-methyl-morpholine; sodium hydride; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In N,N-dimethyl-formamide;
DOI:10.1021/ja001547g

Reference yield: 58.0%

: 306956-35-4
2-[[(4-{2-[(1-benzofuran-2-ylcarbonyl)amino]ethoxy}phenyl)sulfonyl](benzyl)amino]-3,5-dimethylbenzoic acid

: 307002-73-9
WAY-170523

Guidance literature:: 2-[[(4-{2-[(1-benzofuran-2-ylcarbonyl)amino]ethoxy}phenyl)sulfonyl](benzyl)amino]-3,5-dimethylbenzoic acid; With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In N,N-dimethyl-formamide; for 1h;

With hydroxylamine hydrochloride; triethylamine; In N,N-dimethyl-formamide; Further stages.;
DOI:10.1021/ja001547g