methyl (2R)-2-methyl-2-(methylsulfonyl)-4-[4-(phenylthio)phenyl]butanoate

Base Information

Chemical Name:methyl (2R)-2-methyl-2-(methylsulfonyl)-4-[4-(phenylthio)phenyl]butanoate
CAS No.:1354546-39-6
Molecular Formula:C₁₉H₂₂O₄S₂
Molecular Weight:378.513
Hs Code.:

Synonyms:methyl (2R)-2-methyl-2-(methylsulfonyl)-4-[4-(phenylthio)phenyl]butanoate

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Chemical Property of methyl (2R)-2-methyl-2-(methylsulfonyl)-4-[4-(phenylthio)phenyl]butanoate

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Technology Process of methyl (2R)-2-methyl-2-(methylsulfonyl)-4-[4-(phenylthio)phenyl]butanoate

There total 5 articles about methyl (2R)-2-methyl-2-(methylsulfonyl)-4-[4-(phenylthio)phenyl]butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1354546-38-5
(3R)-4-(4-methoxy-3-methyl-3-(methylsulfonyl)-4-oxobutyl)phenylboronic acid

: 882-33-7
diphenyldisulfane

: 1354546-39-6
methyl (2R)-2-methyl-2-(methylsulfonyl)-4-[4-(phenylthio)phenyl]butanoate

Guidance literature:: With [2,2]bipyridinyl; copper(l) iodide; In water; dimethyl sulfoxide; at 100 ℃; for 16h;
DOI:10.1021/jm2014748

Reference yield:

: 1354546-84-1
methyl (2R)-4-(4-bromophenyl)-2-methyl-2-(methylsulfonyl)butanoate

: 1354546-39-6
methyl (2R)-2-methyl-2-(methylsulfonyl)-4-[4-(phenylthio)phenyl]butanoate

Guidance literature:: Multi-step reaction with 3 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / 1,4-dioxane / 16 h / Reflux

2: hydrogenchloride; sodium periodate / tetrahydrofuran; water / 16 h / 20 °C

3: [2,2]bipyridinyl; copper(l) iodide / water; dimethyl sulfoxide / 16 h / 100 °C

With hydrogenchloride; [2,2]bipyridinyl; sodium periodate; copper(l) iodide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In tetrahydrofuran; 1,4-dioxane; water; dimethyl sulfoxide;
DOI:10.1021/jm2014748

Reference yield:

: 1354546-85-2
methyl (2R)-2-methyl-2-(methylsulfonyl)-4-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]butanoate

: 1354546-39-6
methyl (2R)-2-methyl-2-(methylsulfonyl)-4-[4-(phenylthio)phenyl]butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; sodium periodate / tetrahydrofuran; water / 16 h / 20 °C

2: [2,2]bipyridinyl; copper(l) iodide / water; dimethyl sulfoxide / 16 h / 100 °C

With hydrogenchloride; [2,2]bipyridinyl; sodium periodate; copper(l) iodide; In tetrahydrofuran; water; dimethyl sulfoxide;
DOI:10.1021/jm2014748