C₃₀H₂₃NO₅

Base Information

• Chemical Name: C₃₀H₂₃NO₅
• CAS No.: 1346896-39-6
• Molecular Formula: C₃₀H₂₃NO₅
• Molecular Weight: 477.516
• Mol file: 1346896-39-6.mol

Synonyms:C₃₀H₂₃NO₅

Chemical Property of C₃₀H₂₃NO₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₂₃NO₅

There total 4 articles about C₃₀H₂₃NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

5,7-bis-benzyloxy-2-oxo-2H-chromene-4-carbaldehyde (17889-09-7) + 4-amino-phenol (123-30-8) → C30H23NO5 (1346896-39-6)

Guidance literature:

In ethanol; for 5h; Reflux;

DOI:10.1016/j.bmcl.2011.09.029

Reference yield:

5,7-bis-benzyloxy-4-methyl-chromen-2-one (17917-62-3) → C30H23NO5 (1346896-39-6)

Guidance literature:

Multi-step reaction with 2 steps

1: selenium(IV) oxide / 5,5-dimethyl-1,3-cyclohexadiene / 20 h / 150 °C

2: ethanol / 5 h / Reflux

With selenium(IV) oxide; In 5,5-dimethyl-1,3-cyclohexadiene; ethanol;

DOI:10.1016/j.bmcl.2011.09.029

Reference yield:

3,5-dihydroxyphenol (108-73-6) → C30H23NO5 (1346896-39-6)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium hydrogensulfate monohydrate / 110 °C

2: potassium carbonate; potassium iodide / acetone / 18 h / 56 °C

3: selenium(IV) oxide / 5,5-dimethyl-1,3-cyclohexadiene / 20 h / 150 °C

4: ethanol / 5 h / Reflux

With selenium(IV) oxide; sodium hydrogensulfate monohydrate; potassium carbonate; potassium iodide; In 5,5-dimethyl-1,3-cyclohexadiene; ethanol; acetone; 1: Pechmann condensation;

DOI:10.1016/j.bmcl.2011.09.029

upstream raw materials:

5,7-bis-benzyloxy-4-methyl-chromen-2-one

5,7-bis-benzyloxy-2-oxo-2H-chromene-4-carbaldehyde

4-amino-phenol

3,5-dihydroxyphenol