C₁₃H₇Cl₃OS

Base Information

• Chemical Name: C₁₃H₇Cl₃OS
• CAS No.: 1416015-41-2
• Molecular Formula: C₁₃H₇Cl₃OS
• Molecular Weight: 317.623
• Mol file: 1416015-41-2.mol

Synonyms:C₁₃H₇Cl₃OS

Chemical Property of C₁₃H₇Cl₃OS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₃H₇Cl₃OS

There total 1 articles about C₁₃H₇Cl₃OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-acetyl-2,5-dichlorothiophene (36157-40-1) + 4-chlorobenzaldehyde (104-88-1) → C13H7Cl3OS (1416015-41-2)

Guidance literature:

With potassium hydroxide; In methanol; at 20 ℃; for 10h;

DOI:10.3390/molecules24224072

Reference yield: 65.0%

C13H7Cl3OS (1416015-41-2) → 5-(4-chlorophenyl)-3-(2,5-dichlorothiophen-3-yl)-4,5-dihydroisoxazole

Guidance literature:

With hydroxylamine hydrochloride; sodium hydroxide; at 75 - 80 ℃; for 3h; Green chemistry;

DOI:10.1007/s00044-014-1016-y

Reference yield: 65.0%

methanol (67-56-1) + C13H7Cl3OS (1416015-41-2) + malononitrile (109-77-3) → 4-(4-chlorophenyl)-2-(2,5-dichlorothiophen-3-yl)-6-methoxypyridine + 4-(4-chlorophenyl)-6-(2,5-dichlorothiophen-3-yl)-2-methoxypyridine-3-carbonitrile

Guidance literature:

for 0.2h; Reflux; Alkaline conditions;

DOI:10.3390/molecules24224072

upstream raw materials:

3-acetyl-2,5-dichlorothiophene

4-chlorobenzaldehyde

Downstream raw materials:

C₂₂H₁₃Cl₄N₃S₂

C₁₄H₁₀Cl₃N₃S₂