1-phenyl-5-[[(3S)-3-[(trityloxy)methyl]pent-4-en-1-yl]thio]-1H-tetrazole

Base Information

Chemical Name:1-phenyl-5-[[(3S)-3-[(trityloxy)methyl]pent-4-en-1-yl]thio]-1H-tetrazole
CAS No.:1373344-90-1
Molecular Formula:C₃₂H₃₀N₄OS
Molecular Weight:518.682
Hs Code.:

Synonyms:1-phenyl-5-[[(3S)-3-[(trityloxy)methyl]pent-4-en-1-yl]thio]-1H-tetrazole

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Chemical Property of 1-phenyl-5-[[(3S)-3-[(trityloxy)methyl]pent-4-en-1-yl]thio]-1H-tetrazole

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Technology Process of 1-phenyl-5-[[(3S)-3-[(trityloxy)methyl]pent-4-en-1-yl]thio]-1H-tetrazole

There total 2 articles about 1-phenyl-5-[[(3S)-3-[(trityloxy)methyl]pent-4-en-1-yl]thio]-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1373344-89-8
(3S)-3-[(trityloxy)methyl]pent-4-en-1-ol

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: 1373344-90-1
1-phenyl-5-[[(3S)-3-[(trityloxy)methyl]pent-4-en-1-yl]thio]-1H-tetrazole

Guidance literature:: With tributylphosphine; diethylazodicarboxylate; In tetrahydrofuran; toluene; at 0 ℃; for 2h;
DOI:10.1021/jo300519g

Reference yield:

: 943902-73-6
(+)-(S)-methyl 3-[(trityloxy)methyl]pent-4-enoate

: 1373344-90-1
1-phenyl-5-[[(3S)-3-[(trityloxy)methyl]pent-4-en-1-yl]thio]-1H-tetrazole

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 1 h / -55 °C

2: tributylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 2 h / 0 °C

With tributylphosphine; diisobutylaluminium hydride; diethylazodicarboxylate; In tetrahydrofuran; hexane; toluene; 2: Mitsunobu reaction;
DOI:10.1021/jo300519g

Reference yield: 81.0%

: 1373344-90-1
1-phenyl-5-[[(3S)-3-[(trityloxy)methyl]pent-4-en-1-yl]thio]-1H-tetrazole

: 1373344-91-2
1-phenyl-5-[[(3S)-3-[(trityloxy)methyl]pent-4-en-1-yl]-sulfonyl]-1H-tetrazole

Guidance literature:: With hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide; In ethanol; water; ethyl acetate; at 20 ℃; for 24h;
DOI:10.1021/jo300519g