C₅₅H₆₃ClN₄O₁₈

Base Information

Chemical Name:C₅₅H₆₃ClN₄O₁₈
CAS No.:223572-41-6
Molecular Formula:C₅₅H₆₃ClN₄O₁₈
Molecular Weight:1103.57
Hs Code.:

C<sub>55</sub>H<sub>63</sub>ClN<sub>4</sub>O<sub>18</sub>

Synonyms:C₅₅H₆₃ClN₄O₁₈

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Chemical Property of C₅₅H₆₃ClN₄O₁₈

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Technology Process of C₅₅H₆₃ClN₄O₁₈

There total 8 articles about C₅₅H₆₃ClN₄O₁₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 223572-33-6
C₆₁H₇₇ClN₄O₁₈Si

: 223572-41-6
C₅₅H₆₃ClN₄O₁₈

Guidance literature:: With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; at 25 ℃; for 6h;
DOI:10.1021/ja992577q

Reference yield:

: 223572-32-5
C₂₂H₃₀BNO₉

: 223572-41-6
C₅₅H₆₃ClN₄O₁₈

Guidance literature:: Multi-step reaction with 2 steps

1: Pd₂(dba)3; (o-tolyl)3P; 1 N aq. Na₂CO₃ / methanol; toluene / 0.25 h / 80 °C

2: 96 percent / Bu₄NF; AcOH / tetrahydrofuran / 6 h / 25 °C

With tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; tetrabutyl ammonium fluoride; sodium carbonate; acetic acid; tris-(o-tolyl)phosphine; In tetrahydrofuran; methanol; toluene; 1: Suzuki coupling / 2: desilylation;
DOI:10.1021/ja992577q

Reference yield:

: 40243-87-6
3,5-dimethoxystyrene

: 223572-41-6
C₅₅H₆₃ClN₄O₁₈

Guidance literature:: Multi-step reaction with 7 steps

1.1: (DHQ)2PHAL; K₂Os₂(OH)4; t-BuOCl / aq. NaOH; propan-1-ol / 0.5 h / 25 °C

2.1: NBS / acetonitrile / 0.5 h / 0 °C

3.1: i-Pr₂NEt / CH₂Cl₂; tetrahydrofuran / 22 h / 25 °C

4.1: i-PrMgBr / 0.5 h / 0 °C

4.2: t-BuLi / -78 °C

4.3: 0.5 h / -78 - 0 °C

5.1: H₂₀

6.1: Pd₂(dba)3; (o-tolyl)3P; 1 N aq. Na₂CO₃ / methanol; toluene / 0.25 h / 80 °C

7.1: 96 percent / Bu₄NF; AcOH / tetrahydrofuran / 6 h / 25 °C

With potassium osmate; N-Bromosuccinimide; Hydroquinone 1,4-phthalazinediyl diether; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; tert-butylhypochlorite; tetrabutyl ammonium fluoride; water; isopropylmagnesium bromide; sodium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; tris-(o-tolyl)phosphine; In tetrahydrofuran; methanol; propan-1-ol; sodium hydroxide; dichloromethane; toluene; acetonitrile; 1.1: asymmetric aminohydroxylation / 2.1: Bromination / 3.1: Alkylation / 4.1: deprotonation / 4.2: Metallation / 4.3: Substitution / 5.1: Hydrolysis / 6.1: Suzuki coupling / 7.1: desilylation;
DOI:10.1021/ja992577q