S-2,4-dimethoxybenzyl toluenethiosulfonate

Base Information

Chemical Name:S-2,4-dimethoxybenzyl toluenethiosulfonate
CAS No.:180712-44-1
Molecular Formula:C₁₆H₁₈O₄S₂
Molecular Weight:338.449
Hs Code.:

Synonyms:S-2,4-dimethoxybenzyl toluenethiosulfonate

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Chemical Property of S-2,4-dimethoxybenzyl toluenethiosulfonate

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Technology Process of S-2,4-dimethoxybenzyl toluenethiosulfonate

There total 3 articles about S-2,4-dimethoxybenzyl toluenethiosulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 7314-44-5
2,4-dimethoxylbenzyl alcohol

: 28519-50-8
potassium thiotosylate

: 180712-44-1
S-2,4-dimethoxybenzyl toluenethiosulfonate

Guidance literature:: 2,4-dimethoxylbenzyl alcohol; With triethylamine; trifluoroacetic anhydride; In dichloromethane; at 0 ℃; for 0.333333h;

potassium thiotosylate; In dichloromethane; acetone; at 20 ℃; for 18h;
DOI:10.1021/ol403288n

Reference yield:

: 7314-44-5
2,4-dimethoxylbenzyl alcohol

: 180712-44-1
S-2,4-dimethoxybenzyl toluenethiosulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 0.08 h / 0 °C

2: CH₂Cl₂; acetone / 18 h / Ambient temperature

With triethylamine; In dichloromethane; acetone;
DOI:10.1016/0040-4020(96)00765-X