Phenyl-acetic acid (1R,2S,6R,7S)-3,5-dioxo-4-aza-tricyclo[5.2.1.0^2,6]dec-8-en-4-yl ester

Base Information

• Chemical Name: Phenyl-acetic acid (1R,2S,6R,7S)-3,5-dioxo-4-aza-tricyclo[5.2.1.0^2,6]dec-8-en-4-yl ester
• CAS No.: 100898-22-4
• Molecular Formula: C₁₇H₁₅NO₄
• Molecular Weight: 297.31

Synonyms:Phenyl-acetic acid (1R,2S,6R,7S)-3,5-dioxo-4-aza-tricyclo[5.2.1.0^2,6]dec-8-en-4-yl ester

Chemical Property of Phenyl-acetic acid (1R,2S,6R,7S)-3,5-dioxo-4-aza-tricyclo[5.2.1.0^2,6]dec-8-en-4-yl ester

Chemical Property:

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Technology Process of Phenyl-acetic acid (1R,2S,6R,7S)-3,5-dioxo-4-aza-tricyclo[5.2.1.0^2,6]dec-8-en-4-yl ester

There total 1 articles about Phenyl-acetic acid (1R,2S,6R,7S)-3,5-dioxo-4-aza-tricyclo[5.2.1.0^2,6]dec-8-en-4-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

phenylacetic acid (103-82-2) + endo-N-hydroxy-5-norbornene-2,3-dicarboxyimide (21715-90-2,397299-61-5) → Phenyl-acetic acid (1R,2S,6R,7S)-3,5-dioxo-4-aza-tricyclo[5.2.1.02,6]dec-8-en-4-yl ester (100898-22-4)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide;

DOI:10.1002/anie.200501399

Reference yield: 75.0%

neomycin A (3947-65-7) + Phenyl-acetic acid (1R,2S,6R,7S)-3,5-dioxo-4-aza-tricyclo[5.2.1.02,6]dec-8-en-4-yl ester (100898-22-4) → N-[(2R,3S,4R,5R,6R)-5-Amino-6-((1R,2R,3S,4R,6S)-4,6-diamino-2,3-dihydroxy-cyclohexyloxy)-3,4-dihydroxy-tetrahydro-pyran-2-ylmethyl]-2-phenyl-acetamide

Guidance literature:

In water; acetonitrile; for 0.5h; sonication;

DOI:10.1002/anie.200501399

upstream raw materials:

phenylacetic acid

endo-N-hydroxy-5-norbornene-2,3-dicarboxyimide

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